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Microwave-assisted pillaring of a montmorillonite with al-polycations in concentrated media
dc.creator | González, Beatriz | es_ES |
dc.creator | Pérez, Alba Helena | es_ES |
dc.creator | Trujillano, Raquel | es_ES |
dc.creator | Gil Bravo, Antonio | es_ES |
dc.creator | Vicente, Miguel Ángel | es_ES |
dc.date.accessioned | 2017-11-15T08:00:45Z | |
dc.date.available | 2017-11-15T08:00:45Z | |
dc.date.issued | 2017 | |
dc.identifier.issn | 1996-1944 (Electronic) | |
dc.identifier.uri | https://hdl.handle.net/2454/26152 | |
dc.description.abstract | A montmorillonite has been intercalated with Al3+ polycations, using concentrated solutions and clay mineral dispersions. The reaction has been assisted by microwave radiation, yielding new intercalated solids and leading to Al-pillared solids after their calcination at 500 °C. The solids were characterized by elemental chemical analysis, X-ray diffraction, FTIR spectroscopy, thermal analyses, and nitrogen adsorption. The evolution of the properties of the materials was discussed as a function of the preparation conditions. Microwave treatment for 2.5 min provided correctly pillared solids. | en |
dc.description.sponsorship | Research projects MAT2013-47811-C2-1-R and MAT2016-78863-C2-R, jointly financed from the Spanish Agencia Estatal de Investigación, AEI (Spanish Ministry of Economy and Competitiveness, MINECO) and the European Regional Development Fund (ERDF). | en |
dc.format.extent | 8 p. | |
dc.format.mimetype | application/pdf | en |
dc.language.iso | eng | en |
dc.publisher | MDPI | en |
dc.relation.ispartof | Materials, 2017, 10(8), 886 | en |
dc.rights | © 2017 by the authors; licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license. | en |
dc.rights.uri | http://creativecommons.org/licenses/by/4.0/ | |
dc.subject | Al-PILC | en |
dc.subject | Keggin polycation | en |
dc.subject | Concentrated media | en |
dc.subject | Microwave radiation | en |
dc.subject | Pillared montmorillonite | en |
dc.title | Microwave-assisted pillaring of a montmorillonite with al-polycations in concentrated media | en |
dc.type | Artículo / Artikulua | es |
dc.type | info:eu-repo/semantics/article | en |
dc.contributor.department | Química Aplicada | es_ES |
dc.contributor.department | Kimika Aplikatua | eu |
dc.rights.accessRights | Acceso abierto / Sarbide irekia | es |
dc.rights.accessRights | info:eu-repo/semantics/openAccess | en |
dc.identifier.doi | 10.3390/ma10080886 | |
dc.relation.projectID | info:eu-repo/grantAgreement/MINECO//MAT2013-47811-C2-1-R/ES/ | en |
dc.relation.projectID | info:eu-repo/grantAgreement/ES/1PE/MAT2016-78863 | en |
dc.relation.publisherversion | https://dx.doi.org/10.3390/ma10080886 | |
dc.type.version | Versión publicada / Argitaratu den bertsioa | es |
dc.type.version | info:eu-repo/semantics/publishedVersion | en |