Ruiz de Galarreta, José Ignacio

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Ruiz de Galarreta

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José Ignacio

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Subject: NIR-HSI ×

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    Mapping acrylamide content in potato chips using near-infrared hyperspectral imaging and chemometrics
    (Elsevier, 2025-03-14) Peraza Alemán, Carlos Miguel; López Maestresalas, Ainara; Jarén Ceballos, Carmen; Ruiz de Galarreta, José Ignacio; Barandalla, Leire; Arazuri Garín, Silvia; Ingeniería; Ingeniaritza; Institute on Innovation and Sustainable Development in Food Chain - ISFOOD
    This study investigated the potential of near-infrared hyperspectral imaging (NIR-HSI) for the prediction of acrylamide content in potato chips. A total of 300 tubers from two potato varieties (Agria and Jaerla) grown in two seasons and processed under the same frying conditions were analysed. Partial Least Square Regression (PLSR) and Support Vector Machine Regression (SVMR), combined with a logarithmic transformation of the acrylamide levels, were applied to develop predictive models. The most optimal outcomes for PLSR yielded R2 p: 0.85, RMSEP: 201 μg/kg and RPD: 2.53, while for SVMR yielded R2 p: 0.80, RMSEP: 229 μg/kg and RPD: 2.22. Furthermore, the selection of significant wavelengths enabled an 87.95 % reduction in variables without affecting the model’s accuracy. Finally, spatial mapping of acrylamide content was conducted on all chips in the external validation set. This method provides both quantification and visualization capabilities, thus enhancing quality control for acrylamide identification in processed potatoes.
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    Predicting the spatial distribution of reducing sugars using near-infrared hyperspectral imaging and chemometrics: a study in multiple potato genotypes
    (Elsevier, 2025-03-27) Peraza Alemán, Carlos Miguel; Arazuri Garín, Silvia; Jarén Ceballos, Carmen; Ruiz de Galarreta, José Ignacio; Barandalla, Leire; López Maestresalas, Ainara; Ingeniería; Ingeniaritza; Institute on Innovation and Sustainable Development in Food Chain - ISFOOD
    The determination of reducing sugars in potatoes is important due to their impact on product quality during industrial processing. The significant variability of these compounds between genotypes presents a challenge to the development of accurate predictive models. This study evaluated the potential of near-infrared hyperspectral imaging (NIR-HSI) for the prediction of reducing sugars in potatoes. For this, a wide range of genotypes (n=92) from two seasons (2020-2021) was selected. Partial Least Squares Regression (PLSR) and Support Vector Machine Regression (SVMR) methods were used to build the prediction models. Furthermore, interval PLS (iPLS), recursive weighted PLS (rPLS), Genetic Algorithm (GA) and Competitive Adaptive Reweighted Sampling (CARS) were used for relevant wavelength identification to develop less computationally complex models. The best full spectrum model (SNV-PLSR) achieved coefficient of determination and root mean square error values of 0.88 and 0.053% and 0.86 and 0.057%, for calibration and external validation, respectively. Variable selection algorithms successfully reduced the dimensionality of the data without compromising the performance of the models. Robust predicted models were built with only 2.65% (CARS-PLSR) and 3.57% (iPLS-SVMR) of the total wavelengths. Finally, a pixel-wise prediction was performed on the validation set and chemical images were built to visualise the spatial distribution of reducing sugars. This study demonstrated that NIR-HSI is a feasible technique for predicting reducing sugars in several potato genotypes.