Open Access
Microstructured optical fiber sensor for soil moisture measurements
(Optical Society of America, 2018) López Aldaba, Aitor; López Torres, Diego; Campo-Bescós, Miguel; López Rodríguez, José Javier; Yerro Lizarazu, David; Elosúa Aguado, César; Arregui San Martín, Francisco Javier; Auguste, Jean-Louis; Jamier, Raphael; Roy, Philippe; López-Amo Sáinz, Manuel; Ingeniaritza Elektrikoa, Elektronikoaren eta Telekomunikazio Ingeniaritzaren; Ingeniaritza; Institute of Smart Cities - ISC; Ingeniería Eléctrica, Electrónica y de Comunicación; Ingeniería
A discrete sensor based on a Sn0₂-FP (Fabry-Pérot) cavity is presented and characterized in real soil conditions. Results are compared, for the first time to our knowledge, with a commercial capacitive sensor and gravimetric measurements.
Open Access
Route towards a label-free optical waveguide sensing platform based on lossy mode resonances
(IFSA Publishing, 2019) Ruiz Zamarreño, Carlos; Zubiate Orzanco, Pablo; Ozcariz Celaya, Aritz; Elosúa Aguado, César; Socorro Leránoz, Abián Bentor; Urrutia Azcona, Aitor; López Torres, Diego; Acha Morrás, Nerea de; Ascorbe Muruzabal, Joaquín; Vitoria Pascual, Ignacio; Imas González, José Javier; Corres Sanz, Jesús María; Díaz Lucas, Silvia; Hernáez Sáenz de Zaitigui, Miguel; Goicoechea Fernández, Javier; Arregui San Martín, Francisco Javier; Matías Maestro, Ignacio; Del Villar, Ignacio; Ingeniaritza Elektrikoa, Elektronikoaren eta Telekomunikazio Ingeniaritzaren; Institute of Smart Cities - ISC; Ingeniería Eléctrica, Electrónica y de Comunicación; Gobierno de Navarra / Nafarroako Gobernua,0011-1365-2017- 000117; Universidad Pública de Navarra / Nafarroako Unibertsitate Publikoa, PJUPNA26
According to recent market studies of the North American company Allied Market Research, the field of photonic sensors is an emerging strategic field for the following years and it is expected to garner $18 billion by 2021. The integration of micro and nanofabrication technologies in the field of sensors has allowed the development of new technological concepts such as lab-on-a-chip which have achieved extraordinary advances in terms of detection and applicability, for example in the field of biosensors. This continuous development has allowed that equipment consisting of many complex devices that occupied a whole room a few years ago, at present it is possible to handle them in the palm of the hand; that formerly long duration processes are carried out in a matter of milliseconds and that a technology previously dedicated solely to military or scientific uses is available to the vast majority of consumers. The adequate combination of micro and nanostructured coatings with optical fiber sensors has permitted us to develop novel sensing technologies, such as the first experimental demonstration of lossy mode resonances (LMRs) for sensing applications, with more than one hundred citations and related publications in high rank journals and top conferences. In fact, fiber optic LMR-based devices have been proven as devices with one of the highest sensitivity for refractometric applications. Refractive index sensitivity is an indirect and simple indicator of how sensitive the device is to chemical and biological species, topic where this proposal is focused. Consequently, the utilization of these devices for chemical and biosensing applications is a clear opportunity that could open novel and interesting research lines and applications as well as simplify current analytical methodologies. As a result, on the basis of our previous experience with LMR based sensors to attain very high sensitivities, the objective of this paper is presenting the route for the development of label-free optical waveguide sensing platform based on LMRs that enable to explore the limits of this technology for bio-chemosensing applications.
Open Access
SnO2-MOF-Fabry-Pérot humidity optical sensor system based on Fast Fourier transform technique
(SPIE, 2016) López Aldaba, Aitor; López Torres, Diego; Ascorbe Muruzabal, Joaquín; Rota Rodrigo, Sergio; Elosúa Aguado, César; López-Amo Sáinz, Manuel; Arregui San Martín, Francisco Javier; Corres Sanz, Jesús María; Auguste, Jean-Louis; Jamier, Raphael; Roy, Philippe; Ingeniaritza Elektrikoa eta Elektronikoa; Institute of Smart Cities - ISC; Ingeniería Eléctrica y Electrónica
In this paper, a new sensor system for relative humidity measurements based on a SnO2 sputtering deposition on a microstructured optical fiber (MOF) low-finesse Fabry-Pérot (FP) sensing head is presented and characterized. The interrogation of the sensing head is carried out by monitoring the Fast Fourier Transform phase variations of the FP interference frequency. This method is low-sensitive to signal amplitude variations and also avoids the necessity of tracking the evolution of peaks and valleys in the spectrum. The sensor is operated within a wide humidity range (20%-90% relative humidity) with a maximum sensitivity achieved of 0.14rad/%. The measurement method uses a commercial optical interrogator as the only active element, this compact solution allows real time analysis of the data.
Open Access
From superhydrophilic to superhydrophobic surfaces by means of polymeric Layer-by-Layer films
(Elsevier, 2015) López Torres, Diego; Elosúa Aguado, César; Hernáez Sáenz de Zaitigui, Miguel; Goicoechea Fernández, Javier; Arregui San Martín, Francisco Javier; Ingeniería Eléctrica y Electrónica; Ingeniaritza Elektrikoa eta Elektronikoa
Open Access
Enhancing sensitivity of photonic crystal fiber interferometric humidity sensor by the thickness of SnO2 thin films
(Elsevier, 2017) López Torres, Diego; Elosúa Aguado, César; Villatoro, Joel; Zubia, Joseba; Rothhardt, Manfred; Schuster, K.; Arregui San Martín, Francisco Javier; Institute of Smart Cities - ISC; Ingeniería Eléctrica y Electrónica; Ingeniaritza Elektrikoa eta Elektronikoa
Open Access
Micro and nanostructured materials for the development of optical fibre sensors
(MDPI, 2017) Elosúa Aguado, César; Arregui San Martín, Francisco Javier; Del Villar, Ignacio; Ruiz Zamarreño, Carlos; Corres Sanz, Jesús María; Bariáin Aisa, Cándido; Goicoechea Fernández, Javier; Hernáez Sáenz de Zaitigui, Miguel; Rivero Fuente, Pedro J.; Socorro Leránoz, Abián Bentor; Urrutia Azcona, Aitor; Sánchez Zábal, Pedro; Zubiate Orzanco, Pablo; López Torres, Diego; Acha Morrás, Nerea de; Ascorbe Muruzabal, Joaquín; Ozcariz Celaya, Aritz; Matías Maestro, Ignacio; Ingeniaritza Elektrikoa eta Elektronikoa; Institute of Smart Cities - ISC; Ingeniería Eléctrica y Electrónica
The measurement of chemical and biomedical parameters can take advantage of the features exclusively offered by optical fibre: passive nature, electromagnetic immunity and chemical stability are some of the most relevant ones. The small dimensions of the fibre generally require that the sensing material be loaded into a supporting matrix whose morphology is adjusted at a nanometric scale. Thanks to the advances in nanotechnology new deposition methods have been developed: they allow reagents from different chemical nature to be embedded into films with a thickness always below a few microns that also show a relevant aspect ratio to ensure a high transduction interface. This review reveals some of the main techniques that are currently been employed to develop this kind of sensors, describing in detail both the resulting supporting matrices as well as the sensing materials used. The main objective is to offer a general view of the state of the art to expose the main challenges and chances that this technology is facing currently.
Open Access
Title enhancement of the sensitivity of a volatile organic compounds MOF-sensor by means of its structure
(MDPI, 2017) López Torres, Diego; López Aldaba, Aitor; Elosúa Aguado, César; Auguste, Jean-Louis; Jamier, Raphael; Roy, Philippe; López-Amo Sáinz, Manuel; Arregui San Martín, Francisco Javier; Ingeniaritza Elektrikoa eta Elektronikoa; Institute for Advanced Materials and Mathematics - INAMAT2; Ingeniería Eléctrica y Electrónica; Universidad Pública de Navarra / Nafarroako Unibertsitate Publikoa
In this paper, we experimentally compare several core structures of Microstructured Optical Fibers (MOFs) for low-finesse Fabry-Pérot (FP) sensors. These sensors are designed for Volatile Organic Compounds (VOCs) measurements. We deposit Indium Tin Oxide (ITO) thin films by sputtering on the MOFs and different optical phase responses of the FP were measured for saturated atmospheres of ethanol. The sensitivity of the developed sensors is demonstrated to depend on the geometry and the dimensions of the MOF-cores. The sensors show recovery times under 100 s and the baselines are fully recovered after exposure to VOC.
Open Access
Relative humidity multi-point optical sensors system based on Fast Fourier multiplexing technique
(SPIE, 2017) López Aldaba, Aitor; López Torres, Diego; Elosúa Aguado, César; Auguste, Jean-Louis; Jamier, Raphael; Roy, Philippe; Arregui San Martín, Francisco Javier; López-Amo Sáinz, Manuel; Ingeniaritza Elektrikoa eta Elektronikoa; Institute of Smart Cities - ISC; Ingeniería Eléctrica y Electrónica
In this paper, a new multipoint optical fiber system for relative humidity measurements based on Sn02-FP (Fabry-Pérot) sensing heads and an optical interrogator as single active device is presented and characterized. The interrogation of the sensing heads is carried out by monitoring the Fast Fourier Transform phase variations of the FP (Fabry-Pérot) interference frequencies. This method allows to multiplex several sensors with different wavelength spacing interference pattern. The sensors operate within a wide humidity range (20%-90% relative humidity) with low crosstalk between them. Five sensing heads have been measured using two different channels of the optical interrogator. The availability of four channels in the interrogator allows to multiplex a higher number of sensors, reducing proportionally the cost of each sensing point.
Open Access
Real time measuring system of multiple chemical parameters using microstructured optical fibers based sensors
(IEEE, 2018) López Aldaba, Aitor; López Torres, Diego; Elosúa Aguado, César; Arregui San Martín, Francisco Javier; Auguste, Jean-Louis; Jamier, Raphael; Roy, Philippe; López-Amo Sáinz, Manuel; Ingeniaritza Elektrikoa, Elektronikoaren eta Telekomunikazio Ingeniaritzaren; Institute of Smart Cities - ISC; Ingeniería Eléctrica, Electrónica y de Comunicación
In this paper, a multiplexing system for simultaneous interrogation of optical fiber sensors which measure different parameters is presented and validated. The whole system has been tested with 6 different sensing heads with different purposes: one temperature sensing head, two relative humidity sensors and three VOCs leak sensors; all of them based on microstructured optical fibers. The interrogation system uses the FFT technique to isolate each sensor's interference, enabling their simultaneous interrogation. The system interrogates all the sensors at frequencies up to 1 KHz, showing a good performance of each measurement without crosstalk between sensors. The developed system is independent of the sensors' purpose or of the multiplexing topology.
Open Access
Contribution to the development of optical fibre sensors based on microstructured optical fibres to detect gases and volatile organic compounds
(2019) López Torres, Diego; Arregui San Martín, Francisco Javier; Elosúa Aguado, César; Ingeniería Eléctrica, Electrónica y de Comunicación; Ingeniaritza Elektrikoa, Elektronikoaren eta Telekomunikazio Ingeniaritzaren; Universidad Pública de Navarra / Nafarroako Unibertsitate Publikoa; Gobierno de Navarra / Nafarroako Gobernua, 2016/PI012
Desde la primera publicación relacionada con las fibras micro estructuradas (MOFs), el desarrollo de sensores basados en fibra óptica (OFSs), que utilizan este tipo de fibras, se ha visto incrementado atrayendo el interés de numerosos grupos de investigación debido al importante papel que juegan en numerosas aplicaciones. Debido a sus propiedades y estructuras únicas, las MOFs son muy útiles en aplicaciones ópticas de sensado, especialmente de gases y compuestos orgánicos volátiles (VOCs). Por estas razones, esta tesis doctoral propone la utilización de este tipo de fibras para generar y desarrollar nuevas estructuras y montajes, capaces de detectar estos parámetros, gases y VOCs. Además, se han realizado diferentes estudios y se han utilizado diferentes técnicas (destacando la transformada rápida de Fourier (FFT) y la multiplexación WDM…), para mejorar las características de los sensores, intentando conseguir de esta manera que el sistema final fuera lo más competitivo posible.