Open Access
SnO2 based optical fiber refractometers
(SPIE, 2012) Sánchez Zábal, Pedro; Ruiz Zamarreño, Carlos; Hernáez Sáenz de Zaitigui, Miguel; Del Villar, Ignacio; Matías Maestro, Ignacio; Arregui San Martín, Francisco Javier; Ingeniería Eléctrica y Electrónica; Ingeniaritza Elektrikoa eta Elektronikoa; Gobierno de Navarra / Nafarroako Gobernua
In this work, the fabrication and characterization of refractometers based on lossy mode resonances (LMR) is presented. Tin dioxide (SnO2) films deposited on optical fibers are used as the LMR supporting coatings. These resonances shift to the red as a function of the external refractive index, enabling the fabrication of robust and highly reproducible wavelength-based optical fiber refractometers. The obtained SnO2-based refractometer shows an average sensitivity of 7198 nm/refractive index unit (RIU) in the range 1.333-1.420 RIU.
Open Access
Lossy mode resonance sensors based on tungsten oxide thin films
(IEEE, 2020) Del Villar, Ignacio; Bohórquez Navarro, Dina Luz; Caputo, Domanico; Buzzin, Alessio; Chiavaioli, Francesco; Baldini, Francesco; Ruiz Zamarreño, Carlos; Matías Maestro, Ignacio; Ingeniaritza Elektrikoa, Elektronikoaren eta Telekomunikazio Ingeniaritzaren; Institute of Smart Cities - ISC; Ingeniería Eléctrica, Electrónica y de Comunicación
Tungsten oxide (WO3) thin-films fabricated on glass slides have been proven to generate lossy mode resonances (LMRs) in the visible region. Obtained devices were characterized in transmission by lateral incidence of light on the edge of glass slides. Resonances at both TE and TM polarizations were analyzed for different thicknesses and in different deposition conditions. Moreover, it was successfully proved that WO3 coated glass slides present a high sensitivity to refractive index, which opens the path to the application of this structure in the domain of optical sensors.
Open Access
Multimode – coreless – multimode fiber-based sensors: theoretical and experimental study
(IEEE, 2019) San Fabián García, Noé; Socorro Leránoz, Abián Bentor; Del Villar, Ignacio; Díaz Lucas, Silvia; Matías Maestro, Ignacio; Ingeniaritza Elektrikoa, Elektronikoaren eta Telekomunikazio Ingeniaritzaren; Institute of Smart Cities - ISC; Ingeniería Eléctrica, Electrónica y de Comunicación
This paper presents a complete study on the spectral behavior of a multimode-coreless-multimode fiber-optic structure, as well as its application as a refractometer and a liquid level sensor. The combination of two standard multimode fibers fused to a coreless fiber segment allows generating narrow interferometric bands in the optical spectrum, whose sensitivity can be improved by an adequate selection of the dimensions of the device (the coreless segment length and the diameter of the sensing area). A second way to improve the performance of the device is to deposit a thin film of SnO2, which allows increasing the sensitivity up to 314 nm/RIU. This widens the number of applications where this structure can be used. As an example, a liquid level sensor with 0.73 nm/mm sensitivity is presented.
Open Access
Monitoring the etching process in LPFGs towards development of highly sensitive sensors
(MDPI, 2017) Del Villar, Ignacio; Cruz, José Luis; Socorro Leránoz, Abián Bentor; Díaz Lucas, Silvia; Corres Sanz, Jesús María; Arregui San Martín, Francisco Javier; Matías Maestro, Ignacio; Ingeniaritza Elektrikoa eta Elektronikoa; Institute for Advanced Materials and Mathematics - INAMAT2; Ingeniería Eléctrica y Electrónica; Gobierno de Navarra / Nafarroako Gobernua: 2016/PI008; Gobierno de Navarra / Nafarroako Gobernua: 2016/PC025; Gobierno de Navarra / Nafarroako Gobernua: 2016/PC026
In this work, the monitoring of the etching process up to a diameter of 30 µm of two LPFG structures has been compared, one of them had initially 125 µm, whereas the second one had 80 µm. By tracking the wavelength shift of the resonance bands during the etching process it is possible to check the quality of etching process (the 80 µm fibre performs better than de 125 µm fibre), and to stop for a specific cladding mode coupling, which permits to obtain an improved sensitivity compared to the initial structure.
Open Access
Lossy mode resonances generated in planar configuration for two-parameter sensing
(IEEE, 2021-04-29) Fuentes Lorenzo, Omar; Corres Sanz, Jesús María; Domínguez Rodríguez, Ismel; Del Villar, Ignacio; Matías Maestro, Ignacio; Ingeniería Eléctrica, Electrónica y de Comunicación; Ingeniaritza Elektrikoa, Elektronikoa eta Telekomunikazio Ingeniaritza; Institute of Smart Cities - ISC
This work shows a new sensor structure for simultaneous measurement of two parameters, temperature and refractive index. The optical configuration consists of incidence of light on the edge of a soda-lime coverslip fully coated with a CuO thin film and partially coated with a PDMS thick layer. This planar configuration permitted to generate two separated lossy mode resonances (LMRs): one centered at 600 nm and the other at 1000 nm. The second resonance is induced by the PDMS layer and it can be used to measure the temperature due to its high thermo-optic coefficient (the sensitivity is -1.75 nm/°C in the temperature range from 20 to 40 °C), whereas the first resonance is used for sensing refractive index with sensitivity of 1460 nm/RIU in the refractive index range from 1.3328 and 1.37. Finally, a calibration test was carried out using a calibrated oil series with refractive index ranging from 1.33 to 1.36. This work demonstrates the possibility of generating multiples resonances in a single structure as simple as a coverslip, which can be used as a multi-parameter interchangeable sensor, especially suitable for biological applications or the detection of heavy metals in water.
Open Access
Generation of lossy mode resonances with different nanocoatings deposited on coverslips
(Optical Society of America, 2020) Fuentes Lorenzo, Omar; Goicoechea Fernández, Javier; Corres Sanz, Jesús María; Del Villar, Ignacio; Ozcariz Celaya, Aritz; Matías Maestro, Ignacio; Ingeniaritza Elektrikoa, Elektronikoaren eta Telekomunikazio Ingeniaritzaren; Institute of Smart Cities - ISC; Ingeniería Eléctrica, Electrónica y de Comunicación
The generation of lossy mode resonances (LMRs) with a setup based on lateral incidence of light in coverslips is a simple platform that can be used for sensing. Here the versatility of this platform is proved by studying the deposition of different coating materials. The devices were characterized with both SEM and AFM microscopy, as well as ellipsometry, which allowed obtaining the main parameters of the coatings (thickness, refractive index and extinction coefficient) and relating them with the different sensitivities to refractive index attained with each material. In this way it was possible to confirm and complete the basic rules observed with lossy mode resonance based optical fiber sensors towards the design of simpler and more compact applications in domains such as chemical sensors or biosensors.
Open Access
Optical fiber refractometers based on indium tin oxide coatings with response in the visible spectral region
(Elsevier, 2011) Ruiz Zamarreño, Carlos; López, S.; Hernáez Sáenz de Zaitigui, Miguel; Del Villar, Ignacio; Matías Maestro, Ignacio; Arregui San Martín, Francisco Javier; Ingeniería Eléctrica y Electrónica; Ingeniaritza Elektrikoa eta Elektronikoa; Gobierno de Navarra / Nafarroako Gobernua
This work presents the fabrication of optical fiber refractometers based on indium tin oxide (ITO) coatings with response in the visible spectral region. ITO thin-films have been sputtered by employing a rotating mechanism that enables the fabrication of smooth homogeneous coatings onto the optical fiber core. The ITO coated optical fiber devices present several resonances in the visible and infra-red region. These resonances show high optical power attenuations (more than 10 dB) in the visible spectral region, which produces changes in the colour of the output visible light. Therefore, since these resonances shift as a function of the surrounding medium refractive index (SMRI), it is feasible to determine the refractive index of the outer medium in contact with the ITO coating by simply monitoring the chromatic coordinates of the visible output light.
Open Access
D-shape optical fiber refractometer based on TM and TE lossy mode resonances
(SPIE, 2014) Zubiate Orzanco, Pablo; Ruiz Zamarreño, Carlos; Del Villar, Ignacio; Matías Maestro, Ignacio; Arregui San Martín, Francisco Javier; Ingeniería Eléctrica, Electrónica y de Comunicación; Ingeniaritza Elektrikoa, Elektronikoa eta Telekomunikazio Ingeniaritza
The fabrication and characterization of an optical fiber refractometer based on Lossy Mode Resonances (LMR) is presented. TiO2/ poly (sodium 4-styrenesulfonate) coatings deposited on side-polished D-shaped optical fibers are used as LMR supporting coatings. LMRs are sensitive to the external medium refractive index and D-shaped optical fibers enable the observation of TE and TM LMR polarizations. These refractometers based on TE and TM LMR showed an average sensitivity of 2737 nm/RIU and 2893 nm/RIU respectively for a surrounding medium refractive index (SMRI) range from 1.35 to 1.41.
Open Access
Multichannel refractometer based on lossy mode resonances
(IEEE, 2022) Fuentes Lorenzo, Omar; Corres Sanz, Jesús María; Domínguez Rodríguez, Ismel; Del Villar, Ignacio; Matías Maestro, Ignacio; Ingeniería Eléctrica, Electrónica y de Comunicación; Ingeniaritza Elektrikoa, Elektronikoaren eta Telekomunikazio Ingeniaritzaren
In this work a new multiparameter sensor platform based on lossy mode resonances is presented. The structure consists of a soda-lime optical slab waveguide butt-coupled to multimode optical fibers. A variable thickness thin-film is deposited to generate multiple independent resonances on the same waveguide, which can be monitored using a single spectrometer. In order to show the potentiality of the structure, a broad resonance was selectively narrowed by etching sections of the LMR producer thin film. The spectral width is progressively reduced, allowing to selectively isolate independent resonances, which opens the path for multiple LMR generation in the same spectra in a multiparameter sensing platform. The experimental results were corroborated with a theoretical analysis based on the finite difference method (FDM). As a proof of concept, two refractometers on the same waveguide were fabricated and tested using PDMS cells. This platform can be easily miniaturized in order to integrate multiple sensors at low cost, what can be of interest for the development of multi-analyte biosensors probes. IEEE
Open Access
Nanodeposition of materials with complex refractive index in long period fiber gratings
(IEEE, 2005) Del Villar, Ignacio; Matías Maestro, Ignacio; Arregui San Martín, Francisco Javier; Achaerandio Alvira, Miguel; Ingeniería Eléctrica y Electrónica; Ingeniaritza Elektrikoa eta Elektronikoa; Gobierno de Navarra / Nafarroako Gobernua
An overlay of higher refractive index than the cladding is deposited on a Long Period Fiber Grating (LPFG). This permits to improve in a great manner the sensitivity of the device to ambient and overlay refractive index changes. This causes large shifts of the attenuation bands in the transmission spectrum. To obtain a maximum sensitivity for specific refractive indices of the overlay and the ambient, an optimum overlay thickness must be selected. If the refractive index of the overlay is complex there is an additional phenomenon of vanishing of the attenuation bands in the transmission spectrum. This occurs for specific thickness values of the overlay. The problem is analyzed with a numerical method based on LP mode approximation and coupled mode theory. Experimental results are contrasted with theoretical ones