Gil Bravo, Antonio

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https://academica-e.unavarra.es/handle/2454/49135

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Gil Bravo

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Antonio

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InaMat2. Instituto de Investigación en Materiales Avanzados y Matemáticas

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0000-0001-9323-5981

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88497

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1806

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Author: González, Beatriz × Subject: Concentrated media ×

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    PublicationOpen Access
    Microwave-assisted pillaring of a montmorillonite with al-polycations in concentrated media
    (MDPI, 2017) González, Beatriz; Pérez, Alba Helena; Trujillano, Raquel; Gil Bravo, Antonio; Vicente, Miguel Ángel; Química Aplicada; Kimika Aplikatua
    A montmorillonite has been intercalated with Al3+ polycations, using concentrated solutions and clay mineral dispersions. The reaction has been assisted by microwave radiation, yielding new intercalated solids and leading to Al-pillared solids after their calcination at 500 °C. The solids were characterized by elemental chemical analysis, X-ray diffraction, FTIR spectroscopy, thermal analyses, and nitrogen adsorption. The evolution of the properties of the materials was discussed as a function of the preparation conditions. Microwave treatment for 2.5 min provided correctly pillared solids.