Open Access
Magnetically activated 3D printable polylactic acid/polycaprolactone/magnetite composites for magnetic induction heating generation
(Springer, 2023) Galarreta Rodríguez, Itziar; López Ortega, Alberto; Garayo Urabayen, Eneko; Beato López, Juan Jesús; La Roca, Paulo Matías; Sánchez-Alarcos Gómez, Vicente; Recarte Callado, Vicente; Gómez Polo, Cristina; Pérez de Landazábal Berganzo, José Ignacio; Ciencias; Zientziak; Institute for Advanced Materials and Mathematics - INAMAT2; Universidad Pública de Navarra / Nafarroako Unibertsitate Publikoa
Additive manufacturing technology has attracted the attention of industrial and technological sectors due to the versatility of the design and the easy manufacture of structural and functional elements based on composite materials. The embedding of magnetic nanoparticles in the polymeric matrix enables the development of an easy manufacturing process of low-cost magnetically active novel polymeric composites. In this work, we report a series of magnetic composites prepared by solution casting method combining 5 to 60 wt.% of 140 ± 50 nm commercial Fe3O4 nanoparticles, with a semi-crystalline, biocompatible, and biodegradable polymeric blend made of polylactic acid (PLA) and polycaprolactone (PCL). The composites were extruded, obtaining 1.5 ± 0.2 mm diameter continuous and flexible filaments for fused deposition modelling 3D printing. The chemical, magnetic, and calorimetric properties of the obtained filaments were investigated by differential scanning calorimetry, thermogravimetric analysis, magnetometry, and scanning electron microscopy. Furthermore, taking advantage of the magnetic character of the filaments, their capability to generate heat under the application of low-frequency alternating magnetic fields (magnetic induction heating) was analyzed. The obtained results expose the versatility of these easy manufacturing and low-cost filaments, where selecting a desired composition, the heating capacity can be properly adjusted for those applications where magnetic induction plays a key role (i.e., magnetic hyperthermia, drug release, heterogeneous catalysis, water electrolysis, gas capture, or materials synthesis).
Open Access
Fast calculation methods for the magnetic field of particle lattices
(AIP Publishing, 2025-02-14) Royo Silvestre, Isaac; Gandía Aguado, David; Beato López, Juan Jesús; Garayo Urabayen, Eneko; Gómez Polo, Cristina; Ciencias; Zientziak; Institute for Advanced Materials and Mathematics - INAMAT2; Estadística, Informática y Matemáticas; Estatistika, Informatika eta Matematika
With the rise of 3D printing and composite materials, components comprising dispersed magnetic particles have become more interesting due to the possibility to design magnetic elements of any shape with varying amounts of the actual magnetic material. However, quick and easy calculation methods are needed to design these components enabling the selection of the optimum required percentage of magnetic particles (millimeter parts contain billions of micro-sized particles). This work proposes a semi-analytical iterative method for the estimation of the magnetic field generated by magnetic composites formed by embedded magnetic particles. The model is compared in terms of accuracy and calculation speed with finite element analysis and the average magnetization model of the magnetic composite. The results are finally supported by the comparison with experimental measurements of the weak magnetic field generated by a magnetic particle lattice.

Garayo Urabayen, Eneko

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