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dc.creatorAlmandoz Sánchez, Eluxkaes_ES
dc.creatorFuentes, Gonzalo G.es_ES
dc.creatorPalacio, José F.es_ES
dc.creatorMartínez de Bujanda Carasusán, Javieres_ES
dc.creatorRodríguez Trías, Rafaeles_ES
dc.date.accessioned2020-11-11T10:25:01Z
dc.date.available2020-11-11T10:25:01Z
dc.date.issued2018
dc.identifier.issn0257-8972
dc.identifier.urihttps://hdl.handle.net/2454/38642
dc.description.abstractThis study reports the synthesis and characterization of ternary Cr-Al-O and quaternary Cr-Al-O-N coatings deposited by cathodic arc physical vapour deposition, for various nitrogen and oxygen mass flow ratios during the growth process. The composition, microstructure, indentation hardness and modulus of the films have been characterized by scanning electron microscopy, electron probe micro-analysis, X-ray diffraction, and nanoindentation techniques. The evolution of the microstructure and mechanical properties of the coatings after ambient air annealing from 800 °C up to 1100 °C have been investigated. As the oxygen to nitrogen mass flow increases, the as-deposited coatings exhibit lower hardness, higher roughness, lower crystallinity and a more marked columnar structure. At oxygen to nitrogen mass flow ratios bigger than 10/90, the coatings exhibit a stoichiometry of the type (CrAl)2+εO3−ε. Only the coatings with an oxygen to nitrogen mass flow ratio smaller than 10/90 retained nitrogen in their compositions. In all cases, the coatings developed a cubic fcc lattice structure. After annealing at 1100 °C the resulting microstructure showed a clear dependency upon the initial composition of the films. The evolution of the microstructure during the high temperature tests, as well as the analysis of the nanoindentation hardness, composition and thickness also provided valuable information about the combined effects of the thermal stability and the oxidation of the deposited coatings.en
dc.description.sponsorshipThis work has been funded by the Spanish Ministry of Economy and Competitiveness through the project PROTEOX MAT2013-45391-P. The European Commission is also acknowledged through the FP7-FOFNMP project MICROFAST under contract Nr 608720. The Research Group of Surface Engineering and Nanostructured Materials in the Universidad Complutense de Madrid also acknowledges financial support of the Spanish MINECO (project MAT2015-65539-P).en
dc.format.extent36 p.
dc.format.mimetypeapplication/pdfen
dc.language.isoengen
dc.publisherElsevieren
dc.relation.ispartofSurface and Coatings Technology, 2018, 351, 153-161en
dc.rights© 2018 Elsevier B.V. This manuscript version is made available under the CC-BY-NC-ND 4.0en
dc.rights.urihttp://creativecommons.org/licenses/by-nc-nd/4.0/
dc.subjectCrAlON coatingsen
dc.subjectWearen
dc.subjectCathodic arc evaporationen
dc.subjectThermal stabilityen
dc.titleChemical and mechanical stability of air annealed cathodic arc evaporated CrAlON coatingsen
dc.typeinfo:eu-repo/semantics/articleen
dc.typeArtículo / Artikuluaes
dc.contributor.departmentIngenieríaes_ES
dc.contributor.departmentIngeniaritzaeu
dc.contributor.departmentInstitute for Advanced Materials and Mathematics - INAMAT2es_ES
dc.rights.accessRightsinfo:eu-repo/semantics/openAccessen
dc.rights.accessRightsAcceso abierto / Sarbide irekiaes
dc.identifier.doi10.1016/j.surfcoat.2018.07.081
dc.relation.projectIDinfo:eu-repo/grantAgreement/MINECO//MAT2013-45391-P/ES/en
dc.relation.projectIDinfo:eu-repo/grantAgreement/MINECO//MAT2015-65539-P/ES/en
dc.relation.projectIDinfo:eu-repo/grantAgreement/European Commission/FP7/608720en
dc.relation.publisherversionhttps://doi.org/10.1016/j.surfcoat.2018.07.081
dc.type.versioninfo:eu-repo/semantics/acceptedVersionen
dc.type.versionVersión aceptada / Onetsi den bertsioaes


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© 2018 Elsevier B.V. This manuscript version is made available under the CC-BY-NC-ND 4.0
La licencia del ítem se describe como © 2018 Elsevier B.V. This manuscript version is made available under the CC-BY-NC-ND 4.0

El Repositorio ha recibido la ayuda de la Fundación Española para la Ciencia y la Tecnología para la realización de actividades en el ámbito del fomento de la investigación científica de excelencia, en la Línea 2. Repositorios institucionales (convocatoria 2020-2021).
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