Artículos de revista DIMEM - MEMIS Aldizkari artikuluak

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Open Access
Surface roughness analysis on the dry turning of an Al-Cu alloy
(Elsevier, 2015) Torres Salcedo, Alexia; Puertas Arbizu, Ignacio; Luis Pérez, Carmelo; Ingeniería Mecánica, Energética y de Materiales; Mekanika, Energetika eta Materialen Ingeniaritza
Nowadays, surface finish has become an important indicator of quality and precision in manufacturing processes and it is considered one of the most important parameter in Industry. In this present study, the influence of different machining parameters on surface roughness has been analyzed. All these parameters have been studied in terms of depth of cut (ap), feed rate (F), cutting speed (Vc) and tool radius (R). A 2030-T4 aluminium alloy has been selected. Moreover, Design of Experiments (DOE) techniques have been used to predict the surface quality in advance and to select the optimal turning conditions. The experimental results revealed that for dry turning operations and for the amplitude parameters, the most significant factor was the interaction effect between the depth of cut and the feed rate. In addition, for facing operations, the feed rate turned out to be the most statistically influential factor of all the surface roughness parameters.
Open Access
Kinematic design of a new four degree-of-freedom parallel robot for knee rehabilitation
(ASME, 2018) Aginaga García, Jokin; Iriarte Goñi, Xabier; Plaza Puértolas, Aitor; Mata, Vicente; Ingeniería Mecánica, Energética y de Materiales; Mekanika, Energetika eta Materialen Ingeniaritza; Institute of Smart Cities - ISC
Rehabilitation robots are increasingly being developed in order to be used by injured people to perform exercise and training. As these exercises do not need wide range movements, some parallel robots with lower mobility architecture can be an ideal solution for this purpose. This paper presents the design of a new four degree-of-freedom (DOF) parallel robot for knee rehabilitation. The required four DOFs are two translations in a vertical plane and two rotations, one of them around an axis perpendicular to the vertical plane and the other one with respect to a vector normal to the instantaneous orientation of the mobile platform. These four DOFs are reached by means of two RPRR limbs and two UPS limbs linked to an articulated mobile platform with an internal DOF. Kinematics of the new mechanism are solved and the direct Jacobian is calculated. A singularity analysis is carried out and the gained DOFs of the direct singularities are calculated. Some of the singularities can be avoided by selecting suitable values of the geometric parameters of the robot. Moreover, among the found singularities, one of them can be used in order to fold up the mechanism for its transportation. It is concluded that the proposed mechanism reaches the desired output movements in order to carry out rehabilitation maneuvers in a singularity-free portion of its workspace.
Open Access
Symbolic multibody methods for real-time simulation of railway vehicles
(Springer, 2018) Ros Ganuza, Javier; Plaza Puértolas, Aitor; Iriarte Goñi, Xabier; Pintor Borobia, Jesús María; Ingeniería Mecánica, Energética y de Materiales; Mekanika, Energetika eta Materialen Ingeniaritza
In this work, recently developed state-of-the-art symbolic multibody methods are tested to accurately model a complex railway vehicle. The model is generated using a symbolic implementation of the principle of virtual power. Creep forces are modeled using a direct symbolic implementation of the standard linear Kalker model. No simplifications, such as base parameter reduction, partial-linearization or lookup tables for contact kinematics, are used. An Implicit–Explicit integration scheme is proposed to efficiently deal with the stiff creep dynamics. Real-time performance is achieved: the CPU time required for a very robust 1 ms integration time step is 203 µs.
Open Access
Determination of the symbolic base inertial parameters of planar mechanisms
(Elsevier, 2017) Iriarte Goñi, Xabier; Ros Ganuza, Javier; Mata, Vicente; Aginaga García, Jokin; Ingeniería Mecánica, Energética y de Materiales; Mekanika, Energetika eta Materialen Ingeniaritza
The inertial information of a planar mechanical system is characterised using 4 inertial parameters per solid. Due to the kinematic constraints, this parametrisation turns out be redundant. In order to reduce the computational cost of the model and make it possible to estimate its inertial parameters, the model is usually written in terms of a minimum set of inertial parameters called base inertial parameters. These parameters completely determine the dynamics of motion (kinetics) of a mechanism and, since their contributions are independent to each other, their actual values can be estimated experimentally. The base inertial parameters expressions can be written as a linear combination of the inertial parameters and determining their symbolic expressions provides a deeper insight into their physical meaning. This paper presents a new algorithm to determine the symbolic expressions of the base inertial parameters of planar mechanisms. The approach is based on a very well known numerical method to obtain the base inertial parameters and on the fact that these parameters belong to a class of functions that lets us search for symbolic expressions matching with them. Since the symbolic expressions are a function of the geometric constants of the system, the presented algorithm constitutes a very valuable tool in design optimisation and it is also very interesting in dynamic parameter estimation, model reduction and other fields.
Open Access
Optical fiber resonance-based pH sensors using gold nanoparticles into polymeric layer-by-layer coatings
(Springer-Verlag, 2016) Arregui San Martín, Francisco Javier; Matías Maestro, Ignacio; Socorro Leránoz, Abián Bentor; Hernáez Sáenz de Zaitigui, Miguel; Goicoechea Fernández, Javier; Rivero Fuente, Pedro J.; Ingeniería Eléctrica y Electrónica; Ingeniaritza Elektrikoa eta Elektronikoa; Ingeniería Mecánica, Energética y de Materiales; Mekanika, Energetika eta Materialen Ingeniaritza
Open Access
Influence of the power supply on the energy efficiency of an alkaline water electrolyser
(Elsevier, 2009) Ursúa Rubio, Alfredo; Marroyo Palomo, Luis; Gubía Villabona, Eugenio; Gandía Pascual, Luis; Diéguez Elizondo, Pedro; Sanchis Gúrpide, Pablo; Ingeniería Eléctrica y Electrónica; Ingeniaritza Elektrikoa eta Elektronikoa; Ingeniería Mecánica, Energética y de Materiales; Mekanika, Energetika eta Materialen Ingeniaritza; Química Aplicada; Kimika Aplikatua; Gobierno de Navarra / Nafarroako Gobernua
Electric energy consumption represents the greatest part of the cost of the hydrogen produced by water electrolysis. An effort is being carried out to reduce this electric consumption and improve the global efficiency of commercial electrolysers. Whereas relevant progresses are being achieved in cell stack configurations and electrodes performance, there are practically no studies on the effect of the electric power supply topology on the electrolyser energy efficiency. This paper presents an analysis on the energy consumption and efficiency of a 1 N m3 h1 commercial alkaline water electrolyser and their dependence on the power supply topology. The different topologies of power supplies are first summarised, analysed and classified into two groups: thyristor-based (ThPS) and transistor-based power supplies (TrPS). An Electrolyser Power Supply Emulator (EPSE) is then designed, developed and satisfactorily validated by means of simulation and experimental tests. With the EPSE, the electrolyser is characterised both obtaining its I–V curves for different temperatures and measuring the useful hydrogen production. The electrolyser is then supplied by means of two different emulated electric profiles that are characteristic of typical ThPS and TrPS. Results show that the cell stack energy consumption is up to 495 W h N m3 lower when it is supplied by the TrPS, which means 10% greater in terms of efficiency.
Open Access
Methodology for energy demand reduction of potato cold storage process
(Wiley, 2022) Sáenz Baños, Mercedes Irache; Latorre Biel, Juan Ignacio; Martínez Cámara, Eduardo; Jiménez Macías, Emilio; Longo, Francesco; Blanco Fernández, Julio; Ingeniería Mecánica, Energética y de Materiales; Mekanika, Energetika eta Materialen Ingeniaritza
In order to maintain the quality of the potatoes over time, it is necessary to store them under certain storage conditions, which minimize losses both of quality and product, preferably without using chemical treatments. Conservation chambers consume a considerable amount of energy. Between 60% and 70% of the electricity consumed is used in refrigeration. Good insulation reduces the need for cooling the potato since its optimum storage temperature for consumption is around 4–7 C and relative humidity is 85%–90%. This research studies potatoes’ cold storage process to minimize the cost in the product value chain and to ensure its competitiveness in the market. A model is developed to assess energy consumption and propose measures to reduce energy, environmental, and economic costs. All this to reduce their impact within the value chain of potato consumption. Practical Applications: In this case study, different energy efficiency measures applied to the cold storage of potatoes have been implemented: replacement or improvement of the performance of refrigeration equipment, insulation and infiltrations in the refrigeration chamber, control of the product entry temperature, thermal conditioning through free-cooling, improvements in lighting equipment, technical management, and supervision of facilities, and thermographic control. The set of actions implemented has allowed to obtain a reduction in energy demand, standardized through the developed reference line, by 16.41% compared to previous years.
Open Access
Environmental impact analysis of natural cork stopper manufacturing
(MDPI, 2022) Flor Montalvo, Francisco Javier; Martínez Cámara, Eduardo; García Alcaraz, Jorge Luis; Jiménez Macías, Emilio; Latorre Biel, Juan Ignacio; Blanco Fernández, Julio; Ingeniería Mecánica, Energética y de Materiales; Mekanika, Energetika eta Materialen Ingeniaritza
For both wine makers and customers, natural cork stoppers are a symbol of quality. More-over, they are essential for maintaining the organoleptic properties of bottled wines throughout their lifespan. This research relied on the life-cycle assessment (LCA) methodology to analyze the relationship between the efficient usage of cork planks and the environmental impact of the cork stopper manufacturing industry. The goals of this research were to analyze and determine the environmental impact of producing 1 kg of natural cork stoppers. The analysis considered cork stoppers of two sizes—24 × 44 mm and 26 × 44 mm—and two manufacturing methods—punching and turning. Our findings indicated that the 24 × 44 mm cork stoppers produced with the punching method had a slightly lower environmental impact (1.36 kg CO2 eq/kg) across the ten analyzed impact categories. Conversely, 26 × 44 mm turned corks had the highest impact on the environment (1.49 kg CO2 eq/kg). Additionally, a comparison of same-sized punched and turned cork stoppers showed that the former had a lower environmental impact. This phenomenon is directly related to plank usage. In conclusion, there is a clear relationship between environmental impact and the efficient usage of raw material. In turn, an efficient usage of raw material depends on both the manufacturing method and stopper size.
Open Access
Influence of maintenance actions in the drying stage of a paper mill on CO2 emissions
(MDPI, 2021) Calvo Herrero, Luis; Domingo, Rosario; Ingeniería Mecánica, Energética y de Materiales; Mekanika, Energetika eta Materialen Ingeniaritza
Greenhouse gases from industrial activities have become a global problem. Emissions management is being developed to raise awareness of the importance of controlling pollution in general and atmospheric emissions in particular. In 2017, the deficit of the rights of issuance in the industrial sectors increased up to 8.3% (verified emissions in 2017 versus allocation in 2017). This trend will increase more at the end of Phase III due to a progressive reduction in allocation. Phase IV will be much more restrictive in allocating emission rights than Phase III. The extra cost of this deficit reinforces the need for industry in general to reduce CO2 and for the paper industry to reduce GHG emissions and generate credits. Old factories are typically identified as sources of pollution in addition to being inefficient compared to new factories. This article discusses the possibilities of-fered by maintenance actions, whose integration into a process can successfully reduce the environmental impact of industrial plants, particularly by reducing the CO2 equivalent emissions (CO2-eq units henceforth CO2) they produce. This case study analyzes the integration of maintenance rules that enable significant thermal energy savings and consequently CO2 emissions reduction associ-ated with papermaking. Managing Key Performance Indicators (KPIs), such as the amount of cold water added to the boiler circuit and the conditions of the air blown into the dryer section hood, can be used as indicators of CO2 emissions generated. The control of the water and temperature reduces these emissions. A defined measure—in this case, t CO2/t Paper—indicates an achievement of a 21% reduction in emissions over the past 8 years.
Open Access
Characterization of two iron bullets from the royal ammunition factory of Eugi (Spain)
(Technical Faculty, University of Belgrade, 2018) Zalakain Iriazabal, Iñaki; Berlanga Labari, Carlos; Álvarez Vega, Lucas; Rivero Fuente, Pedro J.; Valencia Monreal, Javier; Rodríguez Trías, Rafael; Mekanika, Energetika eta Materialen Ingeniaritza; Institute for Advanced Materials and Mathematics - INAMAT2; Ingeniería Mecánica, Energética y de Materiales
In this work, a comparative analysis of two iron bullets found in The Royal Ammunition Factory of Eugi in Navarra (Spain) was performed. Both bullets presented a spherical shape with a relatively good state of preservation, belonging to the last years of the factory production (1766-1850). Several techniques such as microhardness, X-ray fluorescence (XRF), light (LM) and scanning electron microscopy (SEM), optical mission spectroscopy (OES) and energy dispersive X-ray spectroscopy (EDX) analysis were used in order to identify the manufacturing process of the two bullets. The analyses of the microstructures carried out by LM and SEM showed that one bullet was composed of white cast iron with a pearlitic matrix, steadite and graphite; while the other was composed of grey cast iron with a pearlitic matrix, graphite and a low amount of steadite. The chemical analysis of the bullets carried out by OES indicated significant differences in the amount of silicon and phosphorous. The variation in silicon content could suggest that the foundry temperature under oxidizing environment varied during the casting. The SEM and EDX analyses showed both bullets had manganese sulphide inclusions but only one of the bullets exhibited titanium and vanadium inclusions. The microhardness analyses carried out revealed Vickers hardness differences along the diameter. This variation could be explained by the differences in cooling rate along the diameter. Based on the physical characteristics of the bullets and on the obtained results, it can be concluded that one of the bullets could have been used as a grapeshot projectile and the other one as a bullet for ribauldequins. In addition, calcined ore and slag found in this factory were also analysed. The variation found in their chemical composition corroborated that the foundry temperature employed during the manufacturing process was low, the slag being enriched in Si, Al and Mn elements.
Open Access
Influence of a commercial antithrombotic filter on the caval blood flow during neutra and valsalva maneuver
(ASME, 2017) Nicolás, M.; Lucea, B.; Laborda, A.; Peña, Estefanía; Malvè, Mauro; Ingeniería Mecánica, Energética y de Materiales; Mekanika, Energetika eta Materialen Ingeniaritza
Anticoagulants are the treatment of choice for pulmonary embolism. When these fail or are contraindicated, vena cava filters are effective devices for preventing clots from the legs from migrating to the lung. Many uncertainties exist when a filter is inserted, especially during physiological activity such as normal breathing and the Valsalva maneuver. These activities are often connected with filter migration and vena cava damage due to the various related vein geometrical configurations. In this work, we analyzed the response of the vena cava during normal breathing and Valsalva maneuver, for a healthy vena cava and after insertion of a commercial Günther-Tulip® filter. Validated computational fluid dynamics (CFD) and patient specific data are used for analyzing blood flow inside the vena cava during these maneuvers. While during normal breathing, the vena cava flow can be considered almost stationary with a very low pressure gradient, during Valsalva the extravascular pressure compresses the vena cava resulting in a drastic reduction of the vein section, a global flow decrease through the cava but increasing the velocity magnitude. This change in the section is altered by the presence of the filter which forces the section of the vena cava before the renal veins to keep open. The effect of the presence of the filter is investigated during these maneuvers showing changes in wall shear stress and velocity patterns.
Open Access
Experimental bench for hemodynamic study of coronary artery with serial stenoses: fractional flow reserve assessment
(Taylor & Francis, 2017) Coppel, R.; Gómez, A. L.; Finet, G.; Malvè, Mauro; Pettigrew, R. I.; Ingeniería Mecánica, Energética y de Materiales; Mekanika, Energetika eta Materialen Ingeniaritza
The aim of this study was to develop an experimental hemodynamic bench to elucidate the influences of such geometrical parameters on the FFR assessment. As a first approach, the present work was focused on the influence of the severity of S1 and S2.
Open Access
On studying the interaction between different stent models and rabbit tracheal tissue: numerical, endoscopic and histological comparison
(Biomedical Engineering Society, 2016) Chaure, J.; Serrano, C.; Fernández-Parra, Rocío; Peña, Estefanía; Malvè, Mauro; Ingeniería Mecánica, Energética y de Materiales; Mekanika, Energetika eta Materialen Ingeniaritza
Stenting technique is employed worldwide for treating atherosclerotic vessel and tracheal stenosis. Both diseases can be treated by means of metallic stents which present advantages but are affected by the main problem of restenosis of the stented area. In this study we have built a rabbit trachea numerical model and we have analyzed it before and after insertion and opening of two types of commercial stent: a Zilver® FlexTM Stent and a WallStentTM. In experimental parallel work, two types of stent were implanted in 30 New Zealand rabbits divided in two groups of 10 animals corresponding to each stent type and a third group made up of 10 animals without stent. The tracheal wall response was assessed by means of computerized tomography by endoscopy, macroscopic findings and histopathological study 90 days after stent deployment. Three idealized trachea models, one model for each group, were created in order to perform the computational study. The animal model was used to validate the numerical findings and to attempt to find qualitative correlations between numerical and experimental results. Experimental findings such as inflammation, granuloma and abnormal tissue growth, assessed from histomorphometric analyses were compared with derived numerical parameters such as wall shear stress (WSS) and maximum principal stress. The direct comparison of these parameters and the biological response supports the hypothesis that WSS and tensile stresses may lead to a greater tracheal epithelium response within the stented region, with the latter seeming to have the dominant role. This study may be helpful for improving stent design and demonstrates the feasibility offered by in-silico investigated tracheal structural and fluid dynamics.
Open Access
In vitro comparison of Günther Tulip and Celect filters. Testing filtering efficiency and pressure drop
(Elsevier, 2015) Nicolás, M.; Malvè, Mauro; Peña, Estefanía; Martínez, Miguel Ángel; Leask, R.; Ingeniería Mecánica, Energética y de Materiales; Mekanika, Energetika eta Materialen Ingeniaritza
In this study, the trapping ability of the Günther Tulip and Celect inferior vena cava filters was evaluated. Thrombus capture rates of the filters were tested in vitro in horizontal position with thrombus diameters of 3 and 6 mm and tube diameter of 19 mm. The filters were tested in centered and tilted positions. Sets of 30 clots were injected into the model and the same process was repeated 20 times for each different condition simulated. Pressure drop experienced along the system was also measured and the percentage of clots captured was recorded. The Günther Tulip filter showed superiority in all cases, trapping almost 100% of 6 mm clots both in an eccentric and tilted position and trapping 81.7% of the 3 mm clots in a centered position and 69.3% in a maximum tilted position. The efficiency of all filters tested decreased as the size of the embolus decreased and as the filter was tilted. The injection of 6 clots raised the pressure drop to 4.1 mmHg, which is a reasonable value that does not cause the obstruction of blood flow through the system.
Open Access
A theoretical model of the endothelial cell morphology due to different waveforms
(Elsevier, 2015) Sáez, Pablo; Malvè, Mauro; Martínez, Miguel Ángel; Ingeniería Mecánica, Energética y de Materiales; Mekanika, Energetika eta Materialen Ingeniaritza
Endothelial cells are key units in the regulatory biological process of blood vessels. They represent an interface to transmit variations on the fluid dynamic changes. They are able to adapt its cytoskeleton, by means of microtubules reorientation and F-actin reorganization, due to new mechanical environments. Moreover, they are responsible for initiating a huge cascade of biological processes, such as the release of endothelins (ET-1), in charge of the constriction of the vessel and growth factors such as TGF β and PDGF. Although a huge efforts have been made in the experimental characterization and description of these two issues the computational modeling has not gained such an attention. In this work we study the 3D remodeling of endothelial cells based on the main features of blood flow. In particular we study how different oscillatory shear index and the time average wall shear stresses modify the endothelial cell shape. We found our model fitted the experimental works presented before in in vitro studies. We also include our model within a computational fluid dynamics simulation of a carotid artery to evaluate endothelial cell shape index which is a key predictor of atheroma plaque formation. Moreover, our approach can be coupled with models of collagen and smooth muscle cell growth, where remodeling and the associated release of chemical substance are involved.
Open Access
Numerical and experimental study of the fluid flow through a medical device
(Elsevier, 2015) Nicolás, M.; Palero, V. R.; Peña, Estefanía; Arroyo, M. P.; Malvè, Mauro; Ingeniería Mecánica, Energética y de Materiales; Mekanika, Energetika eta Materialen Ingeniaritza
The purpose of this paper is to verify a commercial software based fluid–structure interaction scheme for the inferior vena cava. Vena cava deep thrombosis (TVP) is a potentially deathly disease consequent to pulmonary thromboembolism (TEP). TEP consist in the obstruction of the pulmonary artery due to a blood clot traveling in the cardiovascular system and is treated with anticoagulants and inferior vena cava filters. Flow fields along the vena cava and an antithrombus filter were studied and compared with a Particle Image Velocimetry (PIV) based model to validate the numerical model. The results show that the fluid–structure interaction (FSI) models are valid and can be used to study the deformations in the inferior vena cava wall using patient-specific geometries.
Open Access
Dynamic considerations of heel-strike impact in human gait
(Springer, 2015) Ros Ganuza, Javier; Font-Llagunes, Josep M.; Plaza Puértolas, Aitor; Kövecses, József; Ingeniería Mecánica, Energética y de Materiales; Mekanika, Energetika eta Materialen Ingeniaritza
Based on the impulsive-dynamics formulation, this article presents the analysis of different strategies to regulate the energy dissipation at the heel-strike event in the context of human locomotion. For this purpose, a seven-link 2D human-like multibody model based on anthropometric data is used. The model captures the most relevant dynamic and energetic aspects of the heel-strike event in the sagittal plane. The pre-impact mechanical state of the system, around which the analysis of the heel impact contribution to energy dissipation is performed, is defined based on published data. In the context of the proposed impulsive-dynamics framework, different realistic strategies that the subject can apply to modify the impact dynamics are proposed and analyzed, namely, the trailing ankle push-off, the torso configuration and the degree of joint blocking in the colliding leg. Detailed numerical analysis and discussions are presented to quantify the effects of the mentioned strategies.
Open Access
Influence of metallic die temperature in the solidification of Cu-10%Al-2%Fe alloy
(Walter de Gruyter, 2010) Cenoz Echeverría, Isaac; Ingeniería Mecánica, Energética y de Materiales; Mekanika, Energetika eta Materialen Ingeniaritza
The phases obtained in copper aluminium bronze alloy (Cu-Al10-Fe2) cast into a permanent die were investigated. The parameters examined were the pre-heating temperatures of the die and the graphite coating thickness. The phases α and γ2 were detected as well as the metastable phases β’ and γ’. The intermetallics of the system Fe-Al were obtained in various stoichiometric compositions. The different cooling rates of the casting resulted in two mechanisms of transformation to α grains out of the unstable β phase, one being nucleation and growth producing needle shaped α grains, the other exhibiting a massive transformation to spherical α grains. These two mechanisms determine the changes in the size of the α grains as a result of changes in the cooling rate in its various ranges.
Open Access
Estudio de una fundición nodular mediante mecánica de la fractura
(Consejo Superior de Investigaciones Científicas (CSIC), 1999) Fernández Carrasquilla, Javier; Ríos, Ricardo; Ingeniería Mecánica, Energética y de Materiales; Mekanika, Energetika eta Materialen Ingeniaritza
Se estudia la tenacidad a la fractura de fundiciones de grafito nodular con diferentes matrices y tamaños de celdilla eutéctica. También se estudian las propiedades de tracción, dureza y tenacidad al impacto. Los resultados experimentales se comparan con los mismos parámetros determinados en acero al silicio de composición química similar a la de la matriz de la fundición. El posterior estudio de las superficies de fractura permite establecer ios mecanismos de rotura. El análisis conjunto de los resultados mecánicos y de los estudios fractográficos permiten establecer la influencia del grafito sobre las diversas propiedades mecánicas de la fundición así como sobre los micromecanismos de fractura.
Open Access
Caracterización de escorias metalúrgicas procedentes de yacimientos arqueológicos de Navarra (siglos II a.C.- IV d.C.)
(Consejo Superior de Investigaciones Científicas (CSIC), 2013) Ros Latienda, L.; Fernández Carrasquilla, Javier; Ingeniería Mecánica, Energética y de Materiales; Mekanika, Energetika eta Materialen Ingeniaritza
Desde la Sección de Arqueología del Gobierno de Navarra llegó la propuesta de caracterizar una serie de piezas comprendidas entre el siglo II a.C. y el siglo IV d.C. procedentes de yacimientos arqueológicos de esta provincia con objeto de obtener datos relacionados con la tecnología que las produjo y poder comparar el grado de desarrollo técnico de diferentes épocas y lugares. Interesaba el estudio de estas piezas desde el punto de vista metalúrgico, habiendo entre ellas mayoritariamente escorias metalúrgicas, restos de piezas fabricadas y restos minerales utilizados en la obtención de diversos metales. Además de proceder a su análisis químico mediante técnica de plasma acoplado inductivamente (ICP), se estudiaron seis muestras mediante microscopía óptica, electrónica de barrido y microanálisis por energía dispersiva de rayos X (EDAX) que reveló la composición de zonas amplias de las escorias y finalmente se completó el estudio determinando las fases presentes mediante difracción de rayos X.