Open Access
Labyrinth metasurface for biosensing applications: numerical study on the new paradigm of metageometries
(MDPI, 2019) Jáuregui López, Irati; Rodríguez Ulibarri, Pablo; Kuznetsov, Sergei A.; Quemada Mayoral, Carlos; Beruete Díaz, Miguel; Ingeniaritza Elektrikoa, Elektronikoaren eta Telekomunikazio Ingeniaritzaren; Institute of Smart Cities - ISC; Ingeniería Eléctrica, Electrónica y de Comunicación
The use of metasurfaces operating in the terahertz regime as biosensor devices has attracted increased interest in recent years due to their enhanced sensitivity and more accurate detection capability. Typical designs are based on the replica of relatively simple unit cells, usually called metaatoms. In a previous paper, we proposed a new paradigm for ultrasensitive thin-film sensors based on complex unit cells, called generically metageometries or labyrinth metasurfaces. Here, we extend this concept towards biosensing, evaluating the performance of the labyrinth as a fungi detector. The sensing capabilities are numerically evaluated and a comparison with previous works in this field is performed, showing that metageometries improve the performance compared to metaatoms both in sensitivity and figure of merit, by a factor of more than four. In particular, we find that it is able to detect five fungi elements scattered on the unit cell, equivalent to a concentration of only 0.004/µm2.
Open Access
Metageometries for polycyclic aromatic hydrocarbons detection at THz range in food systems
(IEEE, 2021) Jáuregui López, Irati; Insausti Barrenetxea, Kizkitza; Beriain Apesteguía, María José; Beruete Díaz, Miguel; Ingeniaritza Elektrikoa, Elektronikoaren eta Telekomunikazio Ingeniaritzaren; Institute of Smart Cities - ISC; Institute on Innovation and Sustainable Development in Food Chain - ISFOOD; Ingeniería Eléctrica, Electrónica y de Comunicación
Polycyclic aromatic hydrocarbons, when present in food systems, have been shown to have a detrimental effect on human health, producing carcinogenic elements. So, the implementation of processes for their detection and identification is of vital importance. Nowadays, there are different methodologies for this purpose, but they consist of expensive and time-consuming processes. Due to their enhanced sensitivity and more accurate detection capability, metageometries operating in the terahertz band arise as a new methodology to identify and detect different chemical or biological substances. In this work, we propose a labyrinth metageometry able to detect different polycyclic aromatic hydrocarbons collected in European regulations as the most critical compounds with high experimental sensitivity. Our design is also capable to distinguish between different compounds at the same concentration. This work leads the way to the design of new metastructures able to improve the current detection limits, and thus obtain a new methodology, easier and less time-consuming that the actual methods.
Open Access
THz sensing with anomalous extraordinary optical transmission hole arrays
(MDPI, 2018) Jáuregui López, Irati; Rodríguez Ulibarri, Pablo; Kuznetsov, Sergei A.; Nikolaev, Nazar A.; Beruete Díaz, Miguel; Ingeniaritza Elektrikoa, Elektronikoaren eta Telekomunikazio Ingeniaritzaren; Institute of Smart Cities - ISC; Ingeniería Eléctrica, Electrónica y de Comunicación
Subwavelength hole array (HA) metasurfaces support the so-called extraordinary optical transmission (EOT) resonance that has already been exploited for sensing. In this work, we demonstrate the superior performance of a different resonant regime of HA metasurfaces called anomalous EOT, by doing a thorough numerical and experimental study of its ability in thin-film label-free sensing applications in the terahertz (THz) band. A comprehensive analysis using both the regular and anomalous EOT resonances is done by depositing thin layers of dielectric analyte slabs of different thicknesses on the structures in different scenarios. We carry out a detailed comparison and demonstrate that the best sensing performance is achieved when the structure operates in the anomalous EOT resonance and the analyte is deposited on the non-patterned side of the metasurface, improving by a factor between 2 and 3 the results of the EOT resonance in any of the considered scenarios. This can be explained by the comparatively narrower linewidth of the anomalous EOT resonance. The results presented expand the reach of subwavelength HAs for sensing applications by considering the anomalous EOT regime that is usually overlooked in the literature.
Open Access
Highly efficient focusing of terahertz waves with an ultrathin superoscillatory metalens: experimental demonstration
(Wiley, 2021-05-06) Legaria Lerga, Santiago; Teniente Vallinas, Jorge; Kuznetsov, Sergei A.; Pacheco-Peña, Víctor; Beruete Díaz, Miguel; Institute of Smart Cities - ISC
The performance of an ultrathin (thickness < 0.04λ 0) metasurface superoscillatory lens (metaSOL) is experimentally demonstrated in the terahertz (THz) range. The metaSOL is designed using two different hexagonal unit cells to improve the efficiency and properties of the conventional transparent–opaque zoning approach. The focusing metastructure produces, at a frequency f exp = 295 GHz, a sharp focal spot 8.9λ exp away from its output surface with a transversal resolution of 0.52λ exp (≈25% below the resolution limit imposed by diffraction), a power enhancement of 18.2 dB, and very low side lobe level (−13 dB). Resolution below the diffraction limit is demonstrated in a broad fractional operation bandwidth of 18%. The focusing capabilities of the proposed metaSOL show its potential use in a range of applications such as THz imaging, microscopy, and communications.
Open Access
Experimental realization of an epsilon-near-zero graded-index metalens at terahertz frequencies
(American Physical Society, 2017) Pacheco-Peña, Víctor; Engheta, Nader; Kuznetsov, Sergei A.; Gentselev, Alexandr; Beruete Díaz, Miguel; Ingeniaritza Elektrikoa eta Elektronikoa; Institute of Smart Cities - ISC; Ingeniería Eléctrica y Electrónica
The terahertz band has been historically hindered by the lack of efficient generators and detectors, but a series of recent breakthroughs have helped to effectively close the “terahertz gap.” A rapid development of terahertz technology has been possible thanks to the translation of revolutionary concepts from other regions of the electromagnetic spectrum. Among them, metamaterials stand out for their unprecedented ability to control wave propagation and manipulate electromagnetic response of matter. They have become a workhorse in the development of terahertz devices such as lenses, polarizers, etc., with fascinating features. In particular, epsilon-near-zero (ENZ) metamaterials have attracted much attention in the past several years due to their unusual properties such as squeezing, tunneling, and supercoupling where a wave traveling inside an electrically small channel filled with an ENZ medium can be tunneled through it, reducing reflections and coupling most of its energy. Here, we design and experimentally demonstrate an ENZ graded-index (GRIN) metamaterial lens operating at terahertz with a power enhancement of 16.2 dB, using an array of narrow hollow rectangular waveguides working near their cutoff frequencies. This is a demonstration of an ENZ GRIN device at terahertz and can open the path towards other realizations of similar devices enabling full quasioptical processing of terahertz signals.
Open Access
Labyrinth metasurface absorber for ultra-high-sensitivity terahertz thin film sensing
(Wiley, 2018) Jáuregui López, Irati; Rodríguez Ulibarri, Pablo; Urrutia Azcona, Aitor; Kuznetsov, Sergei A.; Beruete Díaz, Miguel; Ingeniaritza Elektrikoa, Elektronikoaren eta Telekomunikazio Ingeniaritzaren; Institute of Smart Cities - ISC; Ingeniería Eléctrica, Electrónica y de Comunicación
In this work, a labyrinth metasurface sensor operating at the low‐frequency edge of the THz band is presented. Its intricate shape leads to a high electric field confinement on the surface of the structure, resulting in ultrasensitive performance, able to detect samples of the order of tens of nanometers at a wavelength of the order of millimeters (i.e., five orders of magnitude larger). The sensing capabilities of the labyrinth metasurface are evaluated numerically and experimentally by covering the metallic face with tin dioxide (SnO2) thin films with thicknesses ranging from 24 to 345 nm. A redshift of the resonant frequency is observed as the analyte thickness increases, until reaching a thickness of 20 μm, where the response saturates. A maximum sensitivity of more than 800 and a figure of merit near 4500 nm−1 are achieved, allowing discriminating differences in the SnO2 thickness of less than 25 nm, and improving previous works by a factor of 35. This result can open a new paradigm of ultrasensitive devices based on intricate metageometries overcoming the limitations of classical metasurface sensor designs based on periodic metaatoms.
Open Access
Extraordinary THz transmission with a small beam spot: the leaky wave mechanism
(Wiley, 2018) Navarro Cía, Miguel; Pacheco-Peña, Víctor; Kuznetsov, Sergei A.; Beruete Díaz, Miguel; Institute of Smart Cities - ISC
The discovery of extraordinary optical transmission (EOT) through patterned metallic foils in the late 1990s was decisive for the development of plasmonics and cleared the path to employ small apertures for a variety of interesting applications all along the electromagnetic spectrum. However, a typical drawback often found in practical EOT structures is the large size needed to obtain high transmittance peaks. Consequently, practical EOT arrays are usually illuminated using an expanded (mimicking a plane wave) beam. Here, it is shown with numerical and experimental results in the THz range that high transmittance peaks can be obtained even with a reduced illumination spot exciting a small number of holes, provided that the structure has a sufficient number of lateral holes out of the illumination spot. These results shed more light on the prominent role of leaky waves in the underlying physics of EOT and have a direct impact on potential applications.
Open Access
Tripod-loop metasurfaces for terahertz-sensing applications: a comparison
(MDPI, 2020) Jáuregui López, Irati; Orazbayev, Bakhtiyar; Pacheco-Peña, Víctor; Beruete Díaz, Miguel; Ingeniería Eléctrica, Electrónica y de Comunicación; Institute of Smart Cities - ISC; Ingeniaritza Elektrikoa, Elektronikoaren eta Telekomunikazio Ingeniaritzaren
The high electric field intensity achieved on the surface of sensors based on metasurfaces (metasensors) makes them an excellent alternative for sensing applications where the volume of the sample to be identified is tiny (for instance, thin-film sensing devices). Various shapes and geometries have been proposed recently for the design of these metasensors unit-cells (meta-atoms) such as split ring resonators or hole arrays, among others. In this paper, we propose, design, and evaluate two types of tripod metasurfaces with different complexity in their geometry. An in-depth comparison of their performance is presented when using them as thin-film sensor devices. The meta-atoms of the proposed metasensors consist of a simple tripod and a hollow tripod structure. From numerical calculations, it is shown that the best geometry to perform thin-film sensing is the compact hollow tripod (due to the highest electric field on its surface) with a mean sensitivity of 3.72 × 10−5 nm−1. Different modifications are made to this structure to improve this value, such as introducing arms in the design and rotating the metallic pattern 30 degrees. The best sensitivity achieved for extremely thin film analytes (5–25 nm thick) has an average value of 1.42 × 10−4 nm, which translates into an extremely high improvement of 381% with respect to the initial hollow tripod structure. Finally, a comparison with other designs found in the literature shows that our design is at the top of the ranking, improving the overall performance by more than one order of magnitude. These results highlight the importance of using metastructures with more complex geometries so that a higher electric field intensity distribution and, therefore, designs with better performance can be obtained.
Open Access
Labyrinth absorber based on metageometries metasurface for fungi detection
(IEEE, 2020) Jáuregui López, Irati; Rodríguez Ulibarri, Pablo; Kuznetsov, Sergei A.; Beruete Díaz, Miguel; Ingeniería Eléctrica, Electrónica y de Comunicación; Ingeniaritza Elektrikoa, Elektronikoaren eta Telekomunikazio Ingeniaritzaren
In this paper a labyrinth metasurface based in the new paradigm of metageometries is designed to operate in the Terahertz (THz) band as a biosensor. First, a numerical study is carried out to study the performance of the metasurface as a refractometer when working in two different configurations: transmission and reflection. Then, its performance as a fungi detector is evaluated and a comparison with other devices is performed, showing that the sensitivity and Figure of Merit (FOM) can be enhanced by the use of these kind of devices, in comparison with the classical approach of metaatoms. Particularly, the designed structure is able to detect 5 fungi elements arbitrarily distributed on the unit cell, which is equivalent to a concentration of 0.004/μm 2 , improving the results available in the literature by a factor of more than 4.
Open Access
Super-oscillatory metalens at terahertz for enhanced focusing with reduced side lobes
(MDPI, 2018) Legaria Lerga, Santiago; Pacheco-Peña, Víctor; Beruete Díaz, Miguel; Institute of Smart Cities - ISC
In this paper, we design and numerically demonstrate an ultra-thin super-oscillatory metalens with a resolution below the diffraction limit. The zones of the lens are implemented using metasurface concepts with hexagonal unit cells. This way, the transparency and, hence, efficiency is optimized, compared to the conventional transparent–opaque zoning approach that introduces, inevitably, a high reflection in the opaque regions. Furthermore, a novel two-step optimization technique, based on evolutionary algorithms, is developed to reduce the side lobes and boost the intensity at the focus. After the design process, we demonstrate that the metalens is able to generate a focal spot of 0.46λ0 (1.4 times below the resolution limit) at the design focal length of 10λ0 with reduced side lobes (the side lobe level being approximately −11 dB). The metalens is optimized at 0.327 THz, and has been validated with numerical simulations.