Open Access
A comparative study between SMS interferometers and lossy mode resonace optical fiber devices for sensing applications
(SPIE, 2015) Socorro Leránoz, Abián Bentor; Hernáez Sáenz de Zaitigui, Miguel; Del Villar, Ignacio; Corres Sanz, Jesús María; Arregui San Martín, Francisco Javier; Matías Maestro, Ignacio; Ingeniería Eléctrica y Electrónica; Ingeniaritza Elektrikoa eta Elektronikoa; Universidad Pública de Navarra / Nafarroako Unibertsitate Publikoa
Optical fiber sensors are of great interest due to their intrinsic advantages over electronic sensors. In this work, the sensing characteristics of two different and novel optical fiber devices are compared, after simultaneously depositing a thin-film using the layer-by-layer assembly deposition process. The first one is an SMS structure, formed by splicing two single-mode fiber pigtails on both sides of a coreless multimode fiber segment. This structure induces an interferometric phenomenon that generates several attenuation and transmission bands along the spectrum. These bands are sensitive to variations in the surrounding refractive index, although this sensitivity has been enhanced by a TiO2/PSS thin-film. The other device is a 40 mm uncladded segment of a 200 µm-core multimode optical fiber. When coated by a TiO2/PSS thinfilm, part of the light transmitted into the uncladded core is coupled into the thin-film, generating a lossy mode resonance (LMR). The absorption peaks due to these phenomena red-shift as long as the thin-film thickness increases or the external RI becomes higher. The performance of these devices as refractometers and relative humidity sensors are tested. Results show that the LMR-based sensor is more sensitive in both situations, in spite of its lower sensitivity. Particularly, it presents a 7-fold sensitivity enhancement when measuring surrounding medium refractive index changes and a 10-fold sensitivity enhancement when measuring environmental relative humidity. To our knowledge, this is the first time that a comparative study between SMS and LMR sensors is performed.
Open Access
An antibacterial submicron fiber mat with in situ synthesized silver nanoparticles
(Wiley, 2012) Rivero Fuente, Pedro J.; Urrutia Azcona, Aitor; Goicoechea Fernández, Javier; Rodríguez, Yoany; Corres Sanz, Jesús María; Arregui San Martín, Francisco Javier; Matías Maestro, Ignacio; Ingeniería Eléctrica, Electrónica y de Comunicación; Ingeniaritza Elektrikoa, Elektronikoa eta Telekomunikazio Ingeniaritza; Institute of Smart Cities - ISC; Ingeniería; Ingeniaritza; Institute for Advanced Materials and Mathematics - INAMAT2
This work presents an alternative approachfor fabricating electrospun submicron highly hydrophilicfiber mats loaded with silver nanoparticles. These fiber matsshow a high efficient antibacterial behavior, very attractivefor applications like wound healing and skin regenerationprocesses. The fabrication method is divided in two steps.First, poly(acrylic acid) (PAA) and b-cyclodextrin (b-CD)submicron fibers were electrospun and further stabilizedusing a thermal treatment, yielding stable hydrogel-likefibers with diameters ranging from 100 nm up to severalmicrons. In the second step, silver ions were loaded into thefibers and then reduced to silver nanoparticles in-situ. Theelectrospinning parameters were adjusted to achieve thedesired properties of the fiber mat (density, size) and after-wards, the characteristics of the silver nanoparticles(amount, size, aggregation) were tuned by controlling thesilver ion loading mechanism. Highly biocide surfaces wereachieved showing more than 99.99% of killing efficiency.The two-step process improves the reproducibility and tun-ability of the fiber mats. To our knowledge, this is the firsttime that stable hydrogel fibers with a highly biocide behav-ior have been fabricated using electrospinning.
Open Access
Optical sensors based on lossy-mode resonances
(Elsevier Science, 2017) Matías Maestro, Ignacio; Ascorbe Muruzabal, Joaquín; Acha Morrás, Nerea de; López Torres, Diego; Zubiate Orzanco, Pablo; Sánchez Zábal, Pedro; Urrutia Azcona, Aitor; Socorro Leránoz, Abián Bentor; Rivero Fuente, Pedro J.; Hernáez Sáenz de Zaitigui, Miguel; Elosúa Aguado, César; Goicoechea Fernández, Javier; Bariáin Aisa, Cándido; Corres Sanz, Jesús María; Ruiz Zamarreño, Carlos; Arregui San Martín, Francisco Javier; Del Villar, Ignacio; Ingeniería Eléctrica y Electrónica; Ingeniaritza Elektrikoa eta Elektronikoa; Institute of Smart Cities - ISC
Open Access
Influence of waist length in lossy mode resonances generated with coated tapered single mode optical fibers
(IEEE, 2011) Socorro Leránoz, Abián Bentor; Del Villar, Ignacio; Corres Sanz, Jesús María; Arregui San Martín, Francisco Javier; Matías Maestro, Ignacio; Ingeniería Eléctrica y Electrónica; Ingeniaritza Elektrikoa eta Elektronikoa; Universidad Pública de Navarra / Nafarroako Unibertsitate Publikoa
In this work, the generation of electromagnetic resonances due to the deposition of a nanocoating on a tapered single-mode optical fiber is analyzed. The layer-by-layer technique is used to control the thickness of the nanocoating. According to the results that have been obtained, the depth of the resonance depends on the length of the waist region. Variations in the transmitted optical power of 40 dB are observed in just a few layers. This can be considered in the fabrication of both highly sensitive resonance-based sensors and optical filters.
Open Access
Fluorescent sensors for the detection of heavy metal ions in aqueous media
(MDPI, 2019) Acha Morrás, Nerea de; Elosúa Aguado, César; Corres Sanz, Jesús María; Arregui San Martín, Francisco Javier; Ingeniaritza Elektrikoa, Elektronikoaren eta Telekomunikazio Ingeniaritzaren; Institute of Smart Cities - ISC; Ingeniería Eléctrica, Electrónica y de Comunicación
Due to the risks that water contamination implies for human health and environmental protection, monitoring the quality of water is a major concern of the present era. Therefore, in recent years several efforts have been dedicated to the development of fast, sensitive, and selective sensors for the detection of heavy metal ions. In particular, fluorescent sensors have gained in popularity due to their interesting features, such as high specificity, sensitivity, and reversibility. Thus, this review is devoted to the recent advances in fluorescent sensors for the monitoring of these contaminants, and special focus is placed on those devices based on fluorescent aptasensors, quantum dots, and organic dyes.
Open Access
Tunable electro-optic wavelength filter based on lossy-guided mode resonances
(Optical Society of America, 2013) Corres Sanz, Jesús María; Ascorbe Muruzabal, Joaquín; Arregui San Martín, Francisco Javier; Matías Maestro, Ignacio; Ingeniería Eléctrica y Electrónica; Ingeniaritza Elektrikoa eta Elektronikoa
In this work an optical fiber tunable filter based on lossy guided-mode resonances (LGMR) is proposed. It consists of a multilayer structure deposited onto the surface of a plastic cladding removed multimode fiber. The first layer is used to generate the LGMR and to work as the first electrode as well; the second one to tune the filter and the outer layer forms the other electrode. The fabricated filter has demonstrated a good sensitivity to the applied voltage showing a change of the LGMR wavelength of 0.4 nm/V. Among other applications, this filter is intended to be used as electro-optic wavelength filter or modulator.
Open Access
Asymmetrically and symmetrically coated tapered optical fiber for sensing applications
(SPIE, 2015) Del Villar, Ignacio; Socorro Leránoz, Abián Bentor; Corres Sanz, Jesús María; Arregui San Martín, Francisco Javier; Matías Maestro, Ignacio; Ingeniería Eléctrica y Electrónica; Ingeniaritza Elektrikoa eta Elektronikoa
The deposition of a non-metallic thin-film in a symmetrically coated tapered optical fiber leads to the generation of resonances due to guidance of a mode in the thin-film. At certain conditions, the resonances overlap each other, which can be avoided with an asymmetric coated tapered optical fiber, which permits to obtain resonances for TM and TE polarization separately. Numerical results showing the sensitivity to coating thickness and surrounding medium refractive index are also presented for both polarizations.
Open Access
High sensitivity optical fiber pH sensor using poly(acrylic acid) nanofibers
(IEEE, 2013-12-19) Corres Sanz, Jesús María; Arregui San Martín, Francisco Javier; Matías Maestro, Ignacio; Rodríguez García, Yoany; Ingeniería Eléctrica y Electrónica; Ingeniaritza Elektrikoa eta Elektronikoa
In this work a new optical fiber pH sensor based on the deposition of poly(acrylic acid) (PAA) using the electrospinning technique is presented. The optical fiber structure consists of a 4 cm segment of hollow core fiber (50/150¿m) spliced between two standard multimode fibers onto which the nanoweb is deposited. The sensitive layer is a membrane composed by PAA nanofibers deposited onto the surface of an optical fiber. The sensor has a repetitive behavior and low hysteresis in the pH range 4-7, with an average sensitivity of 0,53 dB/pH.
Open Access
Sensors based on thin-film coated cladding removed multimode optical fiber and single-mode multimode single-mode fiber: a comparative study
(Hindawi Publishing Corporation, 2015) Del Villar, Ignacio; Socorro Leránoz, Abián Bentor; Hernáez Sáenz de Zaitigui, Miguel; Corres Sanz, Jesús María; Ruiz Zamarreño, Carlos; Sánchez Zábal, Pedro; Arregui San Martín, Francisco Javier; Matías Maestro, Ignacio; Ingeniería Eléctrica y Electrónica; Ingeniaritza Elektrikoa eta Elektronikoa
Two simple optical fibre structures that do not require the inscription of a grating, a cladding removed multimode optical fibre (CRMOF) and a single-mode multimode single-mode structure (SMS), are compared in terms of their adequateness for sensing once they are coated with thin-films.The thin-film deposited (TiO2/PSS) permits increasing the sensitivity to surrounding medium refractive index. The results obtained can be extrapolated to other fields such as biological or chemical sensing just by replacing the thin-film by a specific material.
Open Access
Dual-cavity fiber fabry-perot interferometer coated with SnO2for relative humidity and temperature sensing
(IEEE, 2020) Domínguez Flores, Carmen E.; Rodríguez-Quiroz, Osvaldo; Monzón-Hernández, David; Ascorbe Muruzabal, Joaquín; Corres Sanz, Jesús María; Arregui San Martín, Francisco Javier; Ingeniaritza Elektrikoa, Elektronikoaren eta Telekomunikazio Ingeniaritzaren; Institute of Smart Cities - ISC; Ingeniería Eléctrica, Electrónica y de Comunicación
An optical fiber tip interferometer for the measurement of relative humidity (RH) and temperature is proposed. The optical fiber structure used, a dual-cavity optical fiber Fabry-Perot interferometer (DFFPI), is simply-to-fabricate, compact, and robust. The reflectance (RDFFPI) of the interferometer is sensitive to the refractive index (RI) and temperature of the external medium. Consequently, when the cross-section of the fiber tip was coated with a SnO 2 thin film, whose RI changes according to the humidity of the surrounding ambient, the measurement of the RH was possible. An increment of the RH produced a decrement of RI of the SnO 2 thin film, then the reflectance of the fiber tip end-face diminished, and this produced a decrement of the visibility of the interference fringes. The analysis of the RDFFPI was carried out in the Fourier domain, using a novel processing method it was possible to establish that the amplitude of two peaks of Fourier spectrum changed at a ratio of 39.49 × 10 -3 %RH -1 in the range of 40 to 90 RH%. On the other hand, the temperature of the humidity chamber was monitored, from 25 to 60 °C at a fixed RH%, by analyzing the phase shift of the interference pattern produced by the changes in the optical path length of the cavities. The good sensitivity, stability, reproducibility, and compactness of the fiber tip RH sensor make this proposal very appealing in a wide range of applications.