Open Access
High sensitivity lossy-mode resonance refractometer using low refractive index PFA planar waveguide
(Elsevier, 2023) Domínguez Rodríguez, Ismel; Corres Sanz, Jesús María; Matías Maestro, Ignacio; Ascorbe Muruzabal, Joaquín; Del Villar, Ignacio; Ingeniería Eléctrica, Electrónica y de Comunicación; Institute of Smart Cities - ISC; Ingeniaritza Elektrikoa, Elektronikoaren eta Telekomunikazio Ingeniaritzaren; Universidad Pública de Navarra / Nafarroako Unibertsitate Publikoa
In this work a new strategy to improve the sensitivity of refractometers based on lossy-mode resonances has been proved. The proximity of the PFA (tetrafluoroethylene-perfluoro polymer) substrate refractive index to that of water has permitted to implement an optical refractometer with a sensitivity of 41,034 nm per refractive index unit (nm/RIU) for refractive indices ranging from 1.3318 to 1.3347. The work is supported with both theoretical and experimental results. This high sensitivity can be used for the development of LMR based chemical sensors and biosensors, where a low limit of detection is required, with the additional advantage of a simple disposable planar configuration.
Open Access
Lossy mode resonance sensors based on lateral light incidence in nanocoated planar waveguides
(Nature Research, 2019) Fuentes Lorenzo, Omar; Del Villar, Ignacio; Corres Sanz, Jesús María; Matías Maestro, Ignacio; Ingeniaritza Elektrikoa, Elektronikoaren eta Telekomunikazio Ingeniaritzaren; Institute of Smart Cities - ISC; Ingeniería Eléctrica, Electrónica y de Comunicación; Gobierno de Navarra / Nafarroako Gobernua, 2018/PC021-022
The deposition of an indium oxide (In2O3) thin film on conventional planar waveguides (a coverslip and a glass slide) allows generating lossy mode resonances (LMR) by lateral incidence of light on the waveguide and by registering the optical spectrum in a spectrometer. This novel sensing system becomes an alternative to optical fibre, the substrate where LMR-based sensors have been developed so far, since it is easier to handle and more robust. An additional advantage is that cost effective waveguides, such as slides or coverslips, can be used in a platform that resembles surface plasmon resonance-based sensors in the Kretschmann configuration but without the need for a coupling prism and with the advantage of being able to generate TE and TM LMR resonances with metallic oxide or polymer thin films. The results are corroborated with simulations, which provide in-depth understanding of the phenomena involved in the sensing system. As a proof-of-concept for the optical platform, two refractometers were developed, one with low sensitivity and for a wide range of refractive indices, and the other with higher sensitivity but for a narrower refractive index range. The sensors presented here open up the path for the development of LMR-based chemical sensors, environmental sensors, biosensors, or even the generation of other optical phenomena with the deposition of multilayer structures, gratings or nanostructures, which is much easier in a planar waveguide than in an optical fibre.
Open Access
Optical fiber immunosensors optimized with cladding etching and ITO nanodeposition
(IEEE, 2018) Cardona-Maya, Yamile; Del Villar, Ignacio; Socorro Leránoz, Abián Bentor; Corres Sanz, Jesús María; Botero-Cadavid, Juan F.; Institute of Smart Cities - ISC; Gobierno de Navarra / Nafarroako Gobernua
Etched optical fiber immunosensors, with and without ITO nanodeposition, have been developed. The performance of these immunosensors has been assessed implementing an immunoassay. The sensitivity of the mmnunosensor increased by a factor of 4 with the ITO nanocoating, whereas the limit of the detection in both types of devices was 0.2 mg/L of antigens in solution.
Open Access
High sensitivity optical fiber pH sensor using poly(acrylic acid) nanofibers
(IEEE, 2013-12-19) Corres Sanz, Jesús María; Arregui San Martín, Francisco Javier; Matías Maestro, Ignacio; Rodríguez García, Yoany; Ingeniería Eléctrica y Electrónica; Ingeniaritza Elektrikoa eta Elektronikoa
In this work a new optical fiber pH sensor based on the deposition of poly(acrylic acid) (PAA) using the electrospinning technique is presented. The optical fiber structure consists of a 4 cm segment of hollow core fiber (50/150¿m) spliced between two standard multimode fibers onto which the nanoweb is deposited. The sensitive layer is a membrane composed by PAA nanofibers deposited onto the surface of an optical fiber. The sensor has a repetitive behavior and low hysteresis in the pH range 4-7, with an average sensitivity of 0,53 dB/pH.
Open Access
Fluorescent sensors for the detection of heavy metal ions in aqueous media
(MDPI, 2019) Acha Morrás, Nerea de; Elosúa Aguado, César; Corres Sanz, Jesús María; Arregui San Martín, Francisco Javier; Ingeniaritza Elektrikoa, Elektronikoaren eta Telekomunikazio Ingeniaritzaren; Institute of Smart Cities - ISC; Ingeniería Eléctrica, Electrónica y de Comunicación
Due to the risks that water contamination implies for human health and environmental protection, monitoring the quality of water is a major concern of the present era. Therefore, in recent years several efforts have been dedicated to the development of fast, sensitive, and selective sensors for the detection of heavy metal ions. In particular, fluorescent sensors have gained in popularity due to their interesting features, such as high specificity, sensitivity, and reversibility. Thus, this review is devoted to the recent advances in fluorescent sensors for the monitoring of these contaminants, and special focus is placed on those devices based on fluorescent aptasensors, quantum dots, and organic dyes.
Open Access
Increasing the sensitivity of an optic level sensor with a wavelength and phase sensitive single-mode multimode single-mode (SMS) fiber structure
(IEEE, 2017) Fuentes Lorenzo, Omar; Del Villar, Ignacio; Vento Álvarez, José Raúl; Socorro Leránoz, Abián Bentor; Gallego Martínez, Elieser Ernesto; Corres Sanz, Jesús María; Matías Maestro, Ignacio; Ingeniaritza Elektrikoa eta Elektronikoa; Institute of Smart Cities - ISC; Ingeniería Eléctrica y Electrónica
The sensitivity of a liquid level sensor based on a single-mode-multimode-single-mode fiber structure has been increased by hydrofluoric acid etching. The etching process was analyzed and monitored both theoretical and experimentally, which permitted to observe that a sinusoidal spectrum can be obtained for low diameters. As an example, a 2.77 fold sensitivity increase was attained by etching from diameter 125 to 50 μm. Moreover, the sinusoidal shape of the optical spectrum permitted to monitor liquid level changes both in wavelength and phase. The cross sensitivity of the sensor to refractive index and temperature was also studied.
Open Access
Etched LPFGs in reflective configuration for sensitivity and attenuation band depth increase
(IEEE, 2016) Del Villar, Ignacio; Socorro Leránoz, Abián Bentor; Corres Sanz, Jesús María; Matías Maestro, Ignacio; Cruz, José Luis; Rego, Gaspar; Ingeniería Eléctrica y Electrónica; Ingeniaritza Elektrikoa eta Elektronikoa
A reflection configuration setup for long-period fiber gratings is presented. It permits to obtain a unique band with attenuation double than that obtained in transmission configuration, which is interesting for applications where this value is reduced (e.g., the mode transition phenomenon). The method is based on the deposition of a silver mirror at the end of the optical fiber, which permits to absorb the power transmitted through cladding modes and to avoid the generation of interferometric bands. The method also solves the requirement of a precise cleave or to polish the end of the grating, a drawback present in other publications. The versatility of the setup has been proved by application of the cladding etching technique until the attenuation band corresponding with the first guided mode in the cladding is visualized in an optical spectrum analyzer. The experimental results are supported by the numerical data obtained with a method based on the exact calculation of core and cladding modes and the utilization of coupled mode theory
Open Access
Optical sensors based on lossy-mode resonances
(Elsevier Science, 2017) Matías Maestro, Ignacio; Ascorbe Muruzabal, Joaquín; Acha Morrás, Nerea de; López Torres, Diego; Zubiate Orzanco, Pablo; Sánchez Zábal, Pedro; Urrutia Azcona, Aitor; Socorro Leránoz, Abián Bentor; Rivero Fuente, Pedro J.; Hernáez Sáenz de Zaitigui, Miguel; Elosúa Aguado, César; Goicoechea Fernández, Javier; Bariáin Aisa, Cándido; Corres Sanz, Jesús María; Ruiz Zamarreño, Carlos; Arregui San Martín, Francisco Javier; Del Villar, Ignacio; Ingeniería Eléctrica y Electrónica; Ingeniaritza Elektrikoa eta Elektronikoa; Institute of Smart Cities - ISC
Open Access
Tunable electro-optic wavelength filter based on lossy-guided mode resonances
(Optical Society of America, 2013) Corres Sanz, Jesús María; Ascorbe Muruzabal, Joaquín; Arregui San Martín, Francisco Javier; Matías Maestro, Ignacio; Ingeniería Eléctrica y Electrónica; Ingeniaritza Elektrikoa eta Elektronikoa
In this work an optical fiber tunable filter based on lossy guided-mode resonances (LGMR) is proposed. It consists of a multilayer structure deposited onto the surface of a plastic cladding removed multimode fiber. The first layer is used to generate the LGMR and to work as the first electrode as well; the second one to tune the filter and the outer layer forms the other electrode. The fabricated filter has demonstrated a good sensitivity to the applied voltage showing a change of the LGMR wavelength of 0.4 nm/V. Among other applications, this filter is intended to be used as electro-optic wavelength filter or modulator.
Open Access
Route towards a label-free optical waveguide sensing platform based on lossy mode resonances
(IFSA Publishing, 2019) Ruiz Zamarreño, Carlos; Zubiate Orzanco, Pablo; Ozcariz Celaya, Aritz; Elosúa Aguado, César; Socorro Leránoz, Abián Bentor; Urrutia Azcona, Aitor; López Torres, Diego; Acha Morrás, Nerea de; Ascorbe Muruzabal, Joaquín; Vitoria Pascual, Ignacio; Imas González, José Javier; Corres Sanz, Jesús María; Díaz Lucas, Silvia; Hernáez Sáenz de Zaitigui, Miguel; Goicoechea Fernández, Javier; Arregui San Martín, Francisco Javier; Matías Maestro, Ignacio; Del Villar, Ignacio; Ingeniaritza Elektrikoa, Elektronikoaren eta Telekomunikazio Ingeniaritzaren; Institute of Smart Cities - ISC; Ingeniería Eléctrica, Electrónica y de Comunicación; Gobierno de Navarra / Nafarroako Gobernua,0011-1365-2017- 000117; Universidad Pública de Navarra / Nafarroako Unibertsitate Publikoa, PJUPNA26
According to recent market studies of the North American company Allied Market Research, the field of photonic sensors is an emerging strategic field for the following years and it is expected to garner $18 billion by 2021. The integration of micro and nanofabrication technologies in the field of sensors has allowed the development of new technological concepts such as lab-on-a-chip which have achieved extraordinary advances in terms of detection and applicability, for example in the field of biosensors. This continuous development has allowed that equipment consisting of many complex devices that occupied a whole room a few years ago, at present it is possible to handle them in the palm of the hand; that formerly long duration processes are carried out in a matter of milliseconds and that a technology previously dedicated solely to military or scientific uses is available to the vast majority of consumers. The adequate combination of micro and nanostructured coatings with optical fiber sensors has permitted us to develop novel sensing technologies, such as the first experimental demonstration of lossy mode resonances (LMRs) for sensing applications, with more than one hundred citations and related publications in high rank journals and top conferences. In fact, fiber optic LMR-based devices have been proven as devices with one of the highest sensitivity for refractometric applications. Refractive index sensitivity is an indirect and simple indicator of how sensitive the device is to chemical and biological species, topic where this proposal is focused. Consequently, the utilization of these devices for chemical and biosensing applications is a clear opportunity that could open novel and interesting research lines and applications as well as simplify current analytical methodologies. As a result, on the basis of our previous experience with LMR based sensors to attain very high sensitivities, the objective of this paper is presenting the route for the development of label-free optical waveguide sensing platform based on LMRs that enable to explore the limits of this technology for bio-chemosensing applications.