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  • PublicationOpen Access
    D-shape optical fiber pH sensor based on lossy mode resonances (LMRs)
    (IEEE, 2016-01-07) Zubiate Orzanco, Pablo; Ruiz Zamarreño, Carlos; Del Villar, Ignacio; Matías Maestro, Ignacio; Arregui San Martín, Francisco Javier; Ingeniería Eléctrica, Electrónica y de Comunicación; Ingeniaritza Elektrikoa, Elektronikoa eta Telekomunikazio Ingeniaritza
    The fabrication and characterization of an optical fiber pH sensor based on Lossy Mode Resonances (LMRs) is presented. PAH/PAA polymeric thin-films fabricated onto side-polished D-shaped optical fibers are used as LMR supporting coatings. The thickness of PAH/PAA coatings can be modified as a function of the external medium pH. As a consequence of this variation, the effective refractive index of the structure will change, producing a shift of the LMR. The fabricated sensor has been used to measure pH from 4.0 to 5.0. This pH sensor showed a sensitivity of 101.3 nm per pH unit, which means a resolution of ~6×10-4 pH units by using a conventional communications Optical Spectrum Analyzer (OSA), which is an improvement over commercial pH sensors.
  • PublicationOpen Access
    D-shape optical fiber refractometer based on TM and TE lossy mode resonances
    (SPIE, 2014) Zubiate Orzanco, Pablo; Ruiz Zamarreño, Carlos; Del Villar, Ignacio; Matías Maestro, Ignacio; Arregui San Martín, Francisco Javier; Ingeniería Eléctrica, Electrónica y de Comunicación; Ingeniaritza Elektrikoa, Elektronikoa eta Telekomunikazio Ingeniaritza
    The fabrication and characterization of an optical fiber refractometer based on Lossy Mode Resonances (LMR) is presented. TiO2/ poly (sodium 4-styrenesulfonate) coatings deposited on side-polished D-shaped optical fibers are used as LMR supporting coatings. LMRs are sensitive to the external medium refractive index and D-shaped optical fibers enable the observation of TE and TM LMR polarizations. These refractometers based on TE and TM LMR showed an average sensitivity of 2737 nm/RIU and 2893 nm/RIU respectively for a surrounding medium refractive index (SMRI) range from 1.35 to 1.41.
  • PublicationOpen Access
    Nanocoated optical fibre for lossy mode resonance (LMR) sensors and filters
    (IEEE, 2015) Del Villar, Ignacio; Arregui San Martín, Francisco Javier; Corres Sanz, Jesús María; Bariáin Aisa, Cándido; Goicoechea Fernández, Javier; Ruiz Zamarreño, Carlos; Elosúa Aguado, César; Hernáez Sáenz de Zaitigui, Miguel; Rivero Fuente, Pedro J.; Socorro Leránoz, Abián Bentor; Urrutia Azcona, Aitor; Sánchez Zábal, Pedro; Zubiate Orzanco, Pablo; López Torres, Diego; Acha Morrás, Nerea de; Ascorbe Muruzabal, Joaquín; Matías Maestro, Ignacio; Ingeniería Eléctrica y Electrónica; Ingeniaritza Elektrikoa eta Elektronikoa
    Nanometer scale coatings with a complex refractive index deposited on optical fibre permit to obtain attenuation bands in the transmission spectrum, whose central wavelength coincides with the moment when a mode guided in the optical fibre cladding starts to be guided in the coating. Due to the complex refractive index of the coating, the guided mode is a lossy mode. Consequently, these attenuation bands receive the name of lossy mode resonances. This phenomenon can be used for development of ultra-high sensitivity photonic devices (for detection, among others, of volatile organic compounds, pH and refractive index) or for optical filtering. In this work, rules for adequate design are indicated based on numerical results obtained with FIMMWAVE and on experimental results that corroborate the theoretical predictions.
  • PublicationOpen Access
    Red de sensores de fibra óptica para la monitorización de nuevos sistemas de cerramientos aplicados en el sector de la construcción
    (Sociedad Española de Optica, 2009) Unzu Ripoll, Ruth; Nazábal Urriza, Juan Antonio; Vargas Silva, Gustavo Adolfo; Hernández, Rufino; Fernández Valdivielso, Carlos; Urriza Ezcurra, Nuria; Galarza Galarza, Marko; Beloqui Eizaguirre, Garbiñe; Yoldi Bengoechea, Alberto; Matías Maestro, Ignacio; Branchi, P.; Borquez, Lorena; López-Amo Sáinz, Manuel; Ingeniería Eléctrica y Electrónica; Ingeniaritza Elektrikoa eta Elektronikoa; Institute of Smart Cities - ISC
    En este trabajo se muestra la monitorización mediante una red de sensores de fibra óptica del cerramiento de una torre de comunicaciones compuesta por nuevos paneles con estructura tipo sándwich alveolar. La monitorización incluye medidas remotas y en tiempo real de 31 sensores de fibra óptica: 20 sensores deformación, 10 sensores de temperatura y un sensor de vibración.
  • PublicationOpen Access
    Fiber-optic pH sensors fabrication based on selective deposition of neutral red
    (IEEE, 2009-01-22) Hernáez Sáenz de Zaitigui, Miguel; Arregui San Martín, Francisco Javier; Matías Maestro, Ignacio; Ruiz Zamarreño, Carlos; Ingeniería Eléctrica y Electrónica; Ingeniaritza Elektrikoa eta Elektronikoa
    In this work, a novel application of the electric field directed layer-by-layer self assembly (EFDLA) selective deposition method for the fabrication of optical fiber pH sensors is presented. Here, indium tin oxide (ITO) coated optical fibers have been fabricated via a dip-coating deposition method. These fibers are used as electrodes in the EFDLA protocol in order to deposit selectively the sensitive layer. Neutral Red (NR) colorimetric pH sensitive indicator and the polymers poly(acrylic acid) (PAA) and poly(allylamine hydrochloride) (PAH) are used in order to obtain a pH sensitive nanostructured coating onto ITO coated optical fibers. The results obtained in this work revealed that the LbL material adsorption on the electrodes can be enhanced or even inhibited when applying a specific direct current voltage between them under some other specific fabrication parameters. Particularly, the response of these sensors to variations of the pH in the surrounding medium was studied when the pH of the solutions used for the fabrication of the films was adjusted to 7.0 and the potential applied between electrodes was set to 2.5 V. These sensors showed fast response time and high repeatability.
  • PublicationOpen Access
    High sensitivity optical fiber pH sensor using poly(acrylic acid) nanofibers
    (IEEE, 2013-12-19) Corres Sanz, Jesús María; Arregui San Martín, Francisco Javier; Matías Maestro, Ignacio; Rodríguez García, Yoany; Ingeniería Eléctrica y Electrónica; Ingeniaritza Elektrikoa eta Elektronikoa
    In this work a new optical fiber pH sensor based on the deposition of poly(acrylic acid) (PAA) using the electrospinning technique is presented. The optical fiber structure consists of a 4 cm segment of hollow core fiber (50/150¿m) spliced between two standard multimode fibers onto which the nanoweb is deposited. The sensitive layer is a membrane composed by PAA nanofibers deposited onto the surface of an optical fiber. The sensor has a repetitive behavior and low hysteresis in the pH range 4-7, with an average sensitivity of 0,53 dB/pH.
  • PublicationOpen Access
    Fiber optic ammonia sensor using Bromocresol Green pH indicator
    (IEEE, 2014-12-15) Rodríguez Rodríguez, Adolfo Josué; May Arrioja, Daniel A.; Domínguez Cruz, René; Ruiz Zamarreño, Carlos; Matías Maestro, Ignacio; Arregui San Martín, Francisco Javier; Ingeniería Eléctrica y Electrónica; Ingeniaritza Elektrikoa eta Elektronikoa
    We report a fiber optic sensor for low levels of ammonia gas detection based on the use a Bromocresol Green (BCG) pH indicator attached to the optical fiber employing hydrophobic and gas permeable polyurethane film named Tecoflex® as attraping matrix. Highly reproducible and reversible fiber optical sensors have been achieved employing simple and short fabrication processes. The advantage for employ a BCG pH indicator is to take advantage of the basicity of ammonia exhibiting a wide spectral response (500 nm-750 nm) and shows recovery times of less than 15 s. The Tecoflex® film provides additional advantages to be measured to the sensitive area of the sensor, such as operation even in extremely dry environments, efficient transport and prevent leakage or detachment of the BCG pH indicator. The combination of the BCG pH indicator and Tecoflex® film provides a reliable and robust fiber optic ammonia gas sensor.
  • PublicationOpen Access
    Nanosensor for detection of glucose
    (SPIE, 2004-06-09) Del Villar, Ignacio; Matías Maestro, Ignacio; Arregui San Martín, Francisco Javier; Ingeniería Eléctrica y Electrónica; Ingeniaritza Elektrikoa eta Elektronikoa
    A novel fibre-optic sensor sensitive to glucose has been designed based on electrostatic self-assembly method. The polycation of the structure is a mixture of poly(allylamine hydrochloride) (PAH) and Prussian Blue, whereas the polyanion is well-known enzyme glucose oxidase (GOx). The range of glucose concentration that can be measured is submilimolar and is located between 0.1 and 2 mM. Measures are based on a new detection scheme based on the slope of the change of signal produced by injection of glucose, yielding to a linear response. The sensor responses in a PH range between 4 and 7.4, which includes the physiological PH of blood. Some rules for estimation of the refractive index of the material deposited and the thickness of bilayers are also given.
  • PublicationOpen Access
    High-resolution absolute-distance measurements using multiple-tunable fiber Bragg gratings
    (SPIE, 2004-06-09) Luquin Rodríguez, Elena; Frazão, Orlando; Ferreira, Luis Alberto; Araújo, Francisco Moita; López-Amo Sáinz, Manuel; Santos, José Luís; Ingeniería Eléctrica y Electrónica; Ingeniaritza Elektrikoa eta Elektronikoa
    We present and demonstrate a high-resolution absolute-distance measurement system based on multiple-wavelength interferometry. The information on a cavity length is obtained by sampling a fringe of its spectral response at different wavelengths. This is achieved by simultaneously tuning multiple fiber Bragg gratings. For a two wavelength system, an unambiguous measurement range of 262 tm was obtained with a resolution of 14.3 nm.
  • PublicationOpen Access
    Molecules assembly toward fiber optic nanosensor development
    (SPIE, 2004-06-09) Matías Maestro, Ignacio; Del Villar, Ignacio; Arregui San Martín, Francisco Javier; Claus, Richard O.; Ingeniería Eléctrica y Electrónica; Ingeniaritza Elektrikoa eta Elektronikoa
    Different optical fiber sensor configurations based on a LBL nano-technique will be presented. With this technique it is possible to fabricate different structures such as nano Fabry Perot interferometers, optical fiber gratings and any other one dimensional photonic bandgap structures that may be used either for sensing applications or for the implementation of other fiber optic devices. Some of the proposed fiber optic sensors have been fabricated and their main characteristics are their negligible temperature dependence, their fast response, the possibility of using low cost LEDs instead of lasers or even the possibility of operating at different wavelengths.
  • PublicationOpen Access
    Optical fiber sensors based on indium tin oxide surface plasmon resonance supporting coatings
    (SPIE, 2009-10-05) Ruiz Zamarreño, Carlos; Hernáez Sáenz de Zaitigui, Miguel; Matías Maestro, Ignacio; Arregui San Martín, Francisco Javier; Ingeniería Eléctrica y Electrónica; Ingeniaritza Elektrikoa eta Elektronikoa
    In this work, surface plasmon resonance (SPR) based optical fiber sensors are revisited by using a transparent conductive coating, Indium Tin Oxide in our case, as the SPR supporting layer. The utilization of these coatings shifts the plasmon resonance band to the infra-red region and allows the tunability of the SPR wavelength by adjusting the film fabrication parameters. Here, we study the fabrication process of these novel devices and characterize their response to variations in the refractive index of the external medium opening the door to a wide range of applications.
  • PublicationOpen Access
    Distortion-free Brillouin distributed sensor using RF shaping of pump pulses
    (SPIE, 2009-10-05) Zornoza Indart, Ander; Olier Aguado, David; Sagüés García, Mikel; Loayssa Lara, Alayn; Ingeniería Eléctrica y Electrónica; Ingeniaritza Elektrikoa eta Elektronikoa
    We demonstrate a novel configuration for Brillouin optical time domain analysis based on single-sideband modulation and RF shaping that provides pump pulses with 80-dB extinction ratio. This extremely reduced leakage, which to our knowledge is the lowest ever achieved, completely suppresses distortion of the measured spectra, thus sensor precision is enhanced. Furthermore, the proposed setup results in a simplified system with only one modulator and no need for optical filtering in detection.
  • PublicationOpen Access
    High sensitive micro-displacement intensity fiber sensor by using a multiwavelength erbium doped fiber ring laser based on optical add-drop multiplexers
    (SPIE, 2014-06-02) Pérez Herrera, Rosa Ana; Leandro González, Daniel; López-Amo Sáinz, Manuel; Ingeniería Eléctrica y Electrónica; Ingeniaritza Elektrikoa eta Elektronikoa
    In this work, a wavelength division multiplexed fiber ring laser, based on optical add-drop multiplexers to interconnect intensity sensors has been experimentally demonstrated. Three different laser lines were obtained simultaneously all with an optical signal to noise ratio higher than 30dB. This proposed configuration is based on commercial devices and is adapted to the ITU channels normative. By using this configuration each sensor was associated with a different wavelength directly offered by each OADM and a reference wavelength was also included in order to distinguish between power variations induced by the transducer or to detect a fiber failure. This sensor system has been experimentally verified by using microbending sensors obtaining experimental slope sensitivity as good as -0.327dB/µm.
  • PublicationOpen Access
    Simultaneous strain and temperature measure based on a single suspended core photonic crystal fiber
    (SPIE, 2014-06-02) Rota Rodrigo, Sergio; López-Amo Sáinz, Manuel; Kobelke, J.; Schuster, K.; Santos, José Luís; Frazão, Orlando; Ingeniería Eléctrica y Electrónica; Ingeniaritza Elektrikoa eta Elektronikoa
    In this work a simultaneous strain and temperature sensor based on a suspended core fiber is proposed. The sensor comprises a 3mm suspended core PCF between SMFs and is based on the combination of two multimodal interferences with different frequency fringe patterns. The interference of the both signal has different sensitivity responses to strain and temperature. Thought a low-pass frequency filtering of the detected spectrum, the wavelength shift of the two interferences can be measured allowing the discrimination of strain and temperature simultaneously. The resolutions of this sensor are 0.45 ºC and 4.02 με.
  • PublicationOpen Access
    Simultaneous measurement of strain and temperature using a unique LPG-coupled fibre laser scheme
    (SPIE, 2014-06-02) Leandro González, Daniel; Ams, Martin; López-Amo Sáinz, Manuel; Sun, Tong; Grattan, Kenneth T. V.; Ingeniería Eléctrica y Electrónica; Ingeniaritza Elektrikoa eta Elektronikoa
    In this work, we present and demonstrate a novel sensor system for simultaneous measurement of strain and temperature through a unique combination of a long period grating (LPG) and a fibre laser based on a fibre Bragg grating (FBG). In order to achieve this, a new erbium doped fibre laser (EDFL) structure is created, showing an optical signal-to-noise ratio (OSNR) of 55 dB and a peak power measured on the OSA between -5 and 0 dBm. The strain and the temperature variation applied on the FBG and the LPG can be monitored through both the fibre laser wavelength shift and the change of the power level of a unique emission line, both showing a clear linear behaviour.
  • PublicationOpen Access
    Fully-switchable multi-wavelength fiber laser based interrogator system for remote and versatile fiber optic sensors multiplexing structures
    (SPIE, 2014-06-02) Bravo Acha, Mikel; Miguel Soto, Verónica de; Ortigosa Cayetano, Amaia; López-Amo Sáinz, Manuel; Ingeniería Eléctrica y Electrónica; Ingeniaritza Elektrikoa eta Elektronikoa
    A novel interrogation system for multiple fiber optic sensor technologies and based on a fully-switchable multiwavelength fiber laser (MWFL) is proposed and experimentally demonstrated. The MWFL can generate any wavelength combination with a minimum emission line distance up to 50 GHz fitting the ITU grid specifications. On the other hand, as proof of concept sensor network, two different networks were multiplexed by using a remote powered by light fiber optic switch. They are based on two different sensor technologies. One of them based on PCF intensity sensors and multiplexed by using an 8 port WDM and the other one based on wavelength temperature/strain FBG sensors.
  • PublicationOpen Access
    Control of the strain sensitivity using a suspended core photonic crystal fiber sensing head
    (SPIE, 2014-06-02) Rota Rodrigo, Sergio; López-Amo Sáinz, Manuel; Kobelke, J.; Schuster, K.; Santos, José Luís; Frazão, Orlando; Ingeniería Eléctrica y Electrónica; Ingeniaritza Elektrikoa eta Elektronikoa
    In this work a strain sensor based on a suspended core fiber is proposed. The sensor comprises a suspended core PCF between SMFs and is based on the multimode interference generated in these transitions. A strain sensitivity study for different sensing heads and stage separation lengths was carried out showing a sensitivity of -2.42 pm/με for the best case. Also the sensing head was tested for curvature and temperature, showing in the first case that it is insensitive to curvature effects, and secondly, that for small sensor lengths it was insensitive to temperature variations.
  • PublicationOpen Access
    Reinforced concrete structural corrosion monitoring using Hi-Bi photonic crystal fibres in a fiber loop structure
    (SPIE, 2014-06-02) Bravo Acha, Mikel; McCague, Colum; Fabian, Matthias; Jaroszewicz, Leszek R.; Mergo, Paweł; Sun, Tong; Grattan, Kenneth T. V.; López-Amo Sáinz, Manuel; Ingeniería Eléctrica, Electrónica y de Comunicación; Ingeniaritza Elektrikoa, Elektronikoa eta Telekomunikazio Ingeniaritza
    A novel sensing approach has been developed for in-situ corrosion monitoring of steel reinforced concrete structures, using an interferometric Sagnac sensor system based on a Hi-Bi photonic crystal fibre (PCF). To do so an accurate fibre alignment procedure has been implemented in order to improve the performance of the sensor system embedded into the concrete structure when it is subjected to an accelerated corrosion test. The positive results obtained have confirmed the effectiveness of such a sensor system for applications in structural health monitoring.
  • PublicationOpen Access
    Compound lasing fiber optic ring resonators for sensing
    (SPIE, 2014-06-02) Rota Rodrigo, Sergio; González Herráez, Miguel; López-Amo Sáinz, Manuel; Ingeniería Eléctrica, Electrónica y de Comunicación; Ingeniaritza Elektrikoa, Elektronikoa eta Telekomunikazio Ingeniaritza
    In this work, we present a new method for increasing simultaneously the sensitivity and interrogation stability of fiberoptic intensity sensors. The configuration is based on a double-coupler ring resonator. On one side, the attenuation sensitivity of the sensor is enhanced by placing it inside a ring resonator. On the other side, the stability of the interrogation method is rendered close to perfect by creating an external lasing ring resonator with matched spectral response. The resulting lasers allow the stable interrogation of the sensors with an impressive sensitivity enhancement. In our experiments, the dynamic range of the intensity sensor (and consequently its sensitivity) is increased 15 dB by using this laser-based interrogation system. Simultaneously, the instability of the system is reduced to ±0.05 dB. In comparison with systems based on external interrogation, our method is >100 times more stable and also simpler, as no wavelength tunable elements are required.
  • PublicationOpen Access
    Quantum dots coatings inside photonic crystal fibers for temperature sensing
    (IEEE, 2008-12-16) Arigita Lasheras, Jesús; Larrión Zabaleta, Beatriz; Bravo Larrea, Javier; Hernáez Sáenz de Zaitigui, Miguel; Matías Maestro, Ignacio; Arregui San Martín, Francisco Javier; Ingeniería Eléctrica, Electrónica y de Comunicación; Ingeniaritza Elektrikoa, Elektronikoa eta Telekomunikazio Ingeniaritza; Gobierno de Navarra / Nafarroako Gobernua
    Temperature sensors based on Quantum Dots (QDs) nanofilms deposited on the inner holes of a Photonic Crystal Fiber (PCF) was created using the layer by layer electrostatic self-assembly method. The structure is based on a PCF fiber segment spliced between two Standard Multimode Fibers (MMF) of different diameters. The sensors showed a linear variation of the intensity and wavelength emission for a temperature range from -20 ºC to 70 ºC.