Open Access
SnO2 based optical fiber refractometers
(SPIE, 2012) Sánchez Zábal, Pedro; Ruiz Zamarreño, Carlos; Hernáez Sáenz de Zaitigui, Miguel; Del Villar, Ignacio; Matías Maestro, Ignacio; Arregui San Martín, Francisco Javier; Ingeniería Eléctrica y Electrónica; Ingeniaritza Elektrikoa eta Elektronikoa; Gobierno de Navarra / Nafarroako Gobernua
In this work, the fabrication and characterization of refractometers based on lossy mode resonances (LMR) is presented. Tin dioxide (SnO2) films deposited on optical fibers are used as the LMR supporting coatings. These resonances shift to the red as a function of the external refractive index, enabling the fabrication of robust and highly reproducible wavelength-based optical fiber refractometers. The obtained SnO2-based refractometer shows an average sensitivity of 7198 nm/refractive index unit (RIU) in the range 1.333-1.420 RIU.
Open Access
Spectral width reduction in lossy mode resonance-based sensors by means of tapered optical fibre structures
(Elsevier, 2014) Socorro Leránoz, Abián Bentor; Del Villar, Ignacio; Corres Sanz, Jesús María; Arregui San Martín, Francisco Javier; Matías Maestro, Ignacio; Ingeniaritza Elektrikoa, Elektronikoaren eta Telekomunikazio Ingeniaritzaren; Institute of Smart Cities - ISC; Ingeniería Eléctrica, Electrónica y de Comunicación
Open Access
Ordered titanium dioxide nanotubes for lossy-mode resonance-based humidity sensing
(Optica Publishing Group, 2022) Pitula, Emil; Kouao, Dujearic-Stephane; Grochowska, Katarzyna; Sezemsky, Petr; Simerova, Radka; Domínguez Rodríguez, Ismel; Siuzdak, Katarzyna; Del Villar, Ignacio; Stranak, Vitezslav; Smietana, Mateusz; Ingeniería Eléctrica, Electrónica y de Comunicación; Ingeniaritza Elektrikoa, Elektronikoaren eta Telekomunikazio Ingeniaritzaren
Ordered titanium dioxide nanotubes on indium tin oxide as a structure supporting lossy-mode resonance is reported. Capability for application of the structure for optical humidity sensing is shown as an application example.
Open Access
High sensitive refractometers based on lossy mode resonances (LMRs) supported by ITO coated D-shaped optical fibers
(Optical Society of America, 2015) Zubiate Orzanco, Pablo; Ruiz Zamarreño, Carlos; Del Villar, Ignacio; Matías Maestro, Ignacio; Arregui San Martín, Francisco Javier; Ingeniería Eléctrica y Electrónica; Ingeniaritza Elektrikoa eta Elektronikoa
Tin doped indium oxide (ITO) coatings fabricated onto D-shaped optical fibers are presented as the supporting medium for Lossy Mode Resonances (LMRs) generation. The characteristic geometry of ITO-coated D-shaped optical fibers enables to observe experimentally LMRs obtained with both TM and TE polarized light (LMRTM and LMRTE). This permits to obtain a maximum transmission decay of 36 dB with a LMR spectral width of 6.9 nm, improving that obtained in previous works, where the LMRs were a combination of an LMRTM and an LMRTE. Surrounding medium refractive index (SMRI) sensitivity characterization of LMRTM has been performed obtaining a maximum sensitivity of 8742 nm/RIU in the range 1.365-1.38 refractive index units (RIU) which overcomes that of surface plasmon resonance-based optical fiber devices presented in recent works.
Open Access
Generation of surface plasmon resonance and lossy mode resonance by thermal treatment of ITO thin-films
(Elsevier, 2014) Del Villar, Ignacio; Ruiz Zamarreño, Carlos; Hernáez Sáenz de Zaitigui, Miguel; Sánchez Zábal, Pedro; Arregui San Martín, Francisco Javier; Matías Maestro, Ignacio; Ingeniería Eléctrica y Electrónica; Ingeniaritza Elektrikoa eta Elektronikoa
Silicon wafers coated with IndiumTinOxide (ITO) by application of sputtering technique have been characterized after different post-annealing techniques, showing that this last factor is critical for the quality of the thin-film and for the creation and tuning of both surface plasmon resonances and lossy mode resonances. By adequate selection of the ITO thin-film thickness both resonances can be tracked in the same spectrum, which can be used in sensor and optical communications fields.
Open Access
Optimization of sensors based on multimode interference in single-mode–multimode– single-mode structure
(IEEE, 2013) Del Villar, Ignacio; Socorro Leránoz, Abián Bentor; Corres Sanz, Jesús María; Arregui San Martín, Francisco Javier; Matías Maestro, Ignacio; Ingeniería Eléctrica y Electrónica; Ingeniaritza Elektrikoa eta Elektronikoa
By coating a single-mode–multimode–single-mode (SMS) structure with a complex refractive index thin-film the central wavelength of the transmission and attenuation bands of the optical spectrum can be shifted. By adequate selection of multimode segment length and diameter, the thin-film thickness and the thin-film refractive index, the sensitivity of the device to the surrounding medium refractive index, the thickness of the thin-film or the refractive index of the thin-film can be optimized. Experimental results are corroborated numerically with the transfer matrix method.
Open Access
Detection of wind turbine gearbox oil degradation with etched single-mode multimode single-mode (SMS) fiber
(Optica, 2018) Del Villar, Ignacio; Goñi Carnicero, Jaime; Arregui San Martín, Francisco Javier; Matías Maestro, Ignacio; Ingeniería Eléctrica, Electrónica y de Comunicación; Ingeniaritza Elektrikoa, Elektronikoa eta Telekomunikazio Ingeniaritza; Institute of Smart Cities - ISC; Gobierno de Navarra / Nafarroako Gobernua
The application of an etching process in a single-mode multimode single-mode (SMS) fiber allows monitoring the change of refractive index of wind turbine gearbox oil due to temperature and degradation. The SMS was designed for operating at short wavelengths, where the setup is less expensive
Open Access
Metallic-dielectric layer based hyperbolic mode resonances in planar waveguides
(IEEE, 2024) González Salgueiro, Lázaro José; Del Villar, Ignacio; Corres Sanz, Jesús María; Goicoechea Fernández, Javier; Matías Maestro, Ignacio; Ingeniería Eléctrica, Electrónica y de Comunicación; Ingeniaritza Elektrikoa, Elektronikoa eta Telekomunikazio Ingeniaritza; Institute of Smart Cities - ISC; Universidad Pública de Navarra / Nafarroako Unibertsitate Publikoa
In this research article, we present a comprehensive investigation into the integration of dielectric and metallic layers on optical waveguides, specifically targeting sensing applications. By utilizing a single bilayer of metal and dielectric on a planar waveguide that meets the conditions of a hyperbolic metamaterial, we significantly enhance the visibility of lossy mode resonances generated with a single dielectric layer, in what can be considered as a hyperbolic mode resonance (HMR), without compromising sensitivity. This improvement leads to an enhanced figure of merit and a reduction of the signal-to-noise ratio. Real-time evolution of spectra during the dielectric layer deposition allows us to establish a map of the multiple phenomena involved, such as surface plasmon resonance, lossy mode resonance, and mode transition. Combining these phenomena in a single structure leads to an unprecedented enhancement in sensing capabilities, demonstrating the potential of dielectric-metallic layer integration on optical waveguides for advanced sensing applications. Moreover, the optimized sensing performance offers promising opportunities for on-chip sensing devices and various applications in biomedicine, environmental monitoring, and chemical analysis.
Open Access
All-fiber ellipsometer for nanoscale dielectric coatings
(Chinese Academy of Sciences, 2023) Imas González, José Javier; Matías Maestro, Ignacio; Del Villar, Ignacio; Ozcariz Celaya, Aritz; Ruiz Zamarreño, Carlos; Albert, Jacques; Ingeniería Eléctrica, Electrónica y de Comunicación; Institute of Smart Cities - ISC; Ingeniaritza Elektrikoa, Elektronikoaren eta Telekomunikazio Ingeniaritzaren
Multiple mode resonance shifts in tilted fiber Bragg gratings (TFBGs) are used to simultaneously measure the thickness and the refractive index of TiO2 thin films formed by Atomic Layer Deposition (ALD) on optical fibers. This is achieved by comparing the experimental wavelength shifts of 8 TFBG resonances during the deposition process with simulated shifts from a range of thicknesses (T) and values of the real part of the refractive index (n). The minimization of an error function computed for each (n, T) pair then provides a solution for the thickness and refractive index of the deposited film and, a posteriori, to verify the deposition rate throughout the process from the time evolution of the wavelength shift data. Validations of the results were carried out with a conventional ellipsometer on flat witness samples deposited simultaneously with the fiber and with scanning electron measurements on cut pieces of the fiber itself. The final values obtained by the TFBG (n = 2.25, final thickness of 185 nm) were both within 4% of the validation measurements. This approach provides a method to measure the formation of nanoscale dielectric coatings on fibers in situ for applications that require precise thicknesses and refractive indices, such as the optical fiber sensor field. Furthermore, the TFBG can also be used as a process monitor for deposition on other substrates for deposition methods that produce uniform coatings on dissimilar shaped substrates, such as ALD.
Open Access
Optical fiber thermo-refractometer
(Optica, 2022) Imas González, José Javier; Ruiz Zamarreño, Carlos; Del Villar, Ignacio; Cardozo da Silva, Jean Carlos; Oliveira, V.; Matías Maestro, Ignacio; Ingeniería Eléctrica, Electrónica y de Comunicación; Ingeniaritza Elektrikoa, Elektronikoaren eta Telekomunikazio Ingeniaritzaren
This work presents the implementation of a thermo-refractometer, which integrates the measurement of both refractive index and temperature in a single optical fiber structure. To this purpose, a lossy mode resonance (LMR)-based refractometer is obtained by means of the deposition of a titanium dioxide (TiO2) thin film onto a side-polished (D-shaped) single mode fiber. Measurement and subsequent temperature compensation are achieved by means of a fiber Bragg grating (FBG) inscribed in the core of the D-shaped region. The LMR wavelength shift is monitored in transmission while the FBG (FBG peak at 1533 nm) displacement is observed in reflection. The LMR is sensitive to both the surrounding refractive index (SRI), with a sensitivity of 3725.2 nm/RIU in the 1.3324-1.3479 range, and the temperature (- 0.186 nm/°C); while the FBG is only affected by the temperature (32.6 pm/°C in the 25°C - 45°C range). With these values, it is possible to recover the SRI and temperature variations from the wavelength shifts of the LMR and the FBG, constituting a thermo-refractometer, where it is suppressed the effect of the temperature over the refractometer operation, which could cause errors in the fourth or even third decimal of the measured SRI value.

Del Villar, Ignacio

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